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Handbook of Thermal Analysis and Calorimetry

Handbook of Thermal Analysis and Calorimetry
Author:
Publisher: Elsevier
Total Pages: 860
Release: 2018-03-12
Genre: Science
ISBN: 0444640630

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Handbook of Thermal Analysis and Calorimetry: Recent Advances, Techniques and Applications, Volume Six, Second Edition, presents the latest in a series that has been well received by the thermal analysis and calorimetry community. This volume covers recent advances in techniques and applications that complement the earlier volumes. There has been tremendous progress in the field in recent years, and this book puts together the most high-impact topics selected for their popularity by new editors Sergey Vyazovkin, Nobuyoshi Koga and Christoph Schick—all editors of Thermochimica Acta. Among the important new techniques covered are biomass conversion; sustainable polymers; polymer nanocompsoties; nonmetallic glasses; phase change materials; propellants and explosives; applications to pharmaceuticals; processes in ceramics, metals, and alloys; ionic liquids; fast-scanning calorimetry, and more. Features 19 all-new chapters to bring readers up to date on the current status of the field Provides a broad overview of recent progress in the most popular techniques and applications Includes chapters authored by a recognized leader in each field and compiled by a new team of editors, each with at least 20 years of experience in the field of thermal analysis and calorimetry Enables applications across a wide range of modern materials, including polymers, metals, alloys, ceramics, energetics and pharmaceutics Overviews the current status of the field and summarizes recent progress in the most popular techniques and applications


Principles of Thermal Analysis and Calorimetry

Principles of Thermal Analysis and Calorimetry
Author: Peter Haines
Publisher: Royal Society of Chemistry
Total Pages: 234
Release: 2007-10-31
Genre: Science
ISBN: 1847551769

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The use of thermal and calorimetric methods has shown rapid growth over the last two decades, in an increasingly wide range of applications. In addition, a number of powerful new techniques have been developed. This book supplies a concise and readable account of the principles, experimental apparatus and practical procedures used in thermal analysis and calorimetric methods of analysis. Brief accounts of the basic theory are reinforced with detailed applications of the methods and contemporary developments. Also included is information on standard test methods and manufacturers. Written by acknowledged experts, Principles of Thermal Analysis and Calorimetry is up-to-date, wide-ranging and practical. It will be an important source of information for many levels of readership in a variety of areas, from students and lecturers through to industrial and laboratory staff and consultants.


Principles of Thermal Analysis and Calorimetry

Principles of Thermal Analysis and Calorimetry
Author: Simon Gaisford
Publisher: Royal Society of Chemistry
Total Pages: 280
Release: 2019-03-15
Genre: Science
ISBN: 1788018133

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The use of thermal and calorimetric methods has shown rapid growth over the past few decades, in an increasingly wide range of applications. The original text was published in 2001; since then there have been significant advances in various analytical techniques and their applications. This second edition supplies an up to date, concise and readable account of the principles, experimental apparatus and practical procedures used in thermal analysis and calorimetric methods of analysis. Written by experts in their field, brief accounts of the basic theory are reinforced with detailed technical advances and contemporary developments. Where appropriate, applications are used to highlight particular operating principles or methods of interpretation. As an important source of information for many levels of readership in a variety of areas, this book will be an aid for students and lecturers through to industrial and laboratory staff and consultants.


Introduction to Thermal Analysis

Introduction to Thermal Analysis
Author: M.E. Brown
Publisher: Springer Science & Business Media
Total Pages: 268
Release: 2006-01-10
Genre: Technology & Engineering
ISBN: 0306484048

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to Thermal Analysis Techniques and Applications Edited by Michael E. Brown Chemistry Department, Rhodes University, Grahamstown, South Africa KLUWER ACADEMIC PUBLISHERS NEW YORK, BOSTON, DORDRECHT, LONDON, MOSCOW eBook ISBN: 0-306-48404-8 Print ISBN: 1-4020-0472-9 ©2004 Kluwer Academic Publishers New York, Boston, Dordrecht, London, Moscow Print ©2001 Kluwer Academic Publishers Dordrecht All rights reserved No part of this eBook may be reproduced or transmitted in any form or by any means, electronic, mechanical, recording, or otherwise, without written consent from the Publisher Created in the United States of America Visit Kluwer Online at: http://kluweronline. com and Kluwer's eBookstore at: http://ebooks. kluweronline. com CONTENTS Preface to the First Edition, Chapman & Hall, London, 1988 ix About the First Edition of this Book x Preface to the Second Edition xi 1. INTRODUCTION 1. 1 Definition and History 1 1. 2 Thermal Analysis Instruments 4 References 11 2. THERMAL EVENTS 2. 1 Introduction 13 2. 2 The Solid State 13 2. 3 Reactions of Solids 14 2. 4 Decomposition of Solids 15 2. 5 Reaction with the Surrounding Atmosphere 16 2. 6 Solid-Solid Interactions 16 References 17 3. THERMOGRAVIMETRY (TG) Introduction 3. 1 19 3. 2 The Balance 19 3. 3 Heating the Sample 21 3. 4 The Atmosphere 24 3. 5 The Sample 26 3. 6 Temperature Measurement 26 3. 7 Temperature Control 28 Sample Controlled Thermal Analysis (SCTA) 29 3. 8 3. 9 Calibration 36 3. 10 Presentation of TG Data 37 3.


Modulated Temperature Differential Scanning Calorimetry

Modulated Temperature Differential Scanning Calorimetry
Author: Mike Reading
Publisher: Springer Science & Business Media
Total Pages: 340
Release: 2006-10-12
Genre: Technology & Engineering
ISBN: 1402037503

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MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of the sample’s heat capacity from the modulation. The new information this provided sparked a revolution in scanning calorimetry by enabling new insights to be gained into almost all aspects of polymer characteristics. This book provides both a basic and advanced treatment of the theory of the technique followed by a detailed exposition of its application to reacting systems, blends and semicrystalline polymers by the leaders in all of these fields. It is an essential text for anybody interested in calorimetry or polymer characterization, especially if they have found that conventional DSC cannot help them with their problems.


Handbook of Thermal Analysis and Calorimetry

Handbook of Thermal Analysis and Calorimetry
Author: Michael E. Brown
Publisher: Elsevier Science
Total Pages: 942
Release: 2003-12-22
Genre: Science
ISBN: 9780444820860

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This is the second volume of a four volume set intended to describe the techniques and applications of thermoanalytical and calorimetric methods. The general techniques and methodology are covered extensively in Volume 1, along with the fundamental physicochemical background needed. Consequently the subsequent volumes dwell on the applications of these powerful and versatile methods, while assuming a familiarity with the techniques. Volume 2 covers major areas of inorganic materials and some related general topics, e.g., catalysis, geochemistry, and the preservation of art. The chapters are written by established practitioners in the field with the intent of presenting a sampling of the how thermoanalytical and calorimetric methods have contributed to progress in their respective areas. The chapters are not intended as exhaustive reviews of the topics, but rather, to illustrate to the readers what has been achieved and to encourage them to consider extending these applications further into their domains of interest. - Provides an appreciation for how thermal methods can be applied to inorganic materials and processes. - Provides an insight into the versatility of thermal methods. - Shares the experiences of experts in a variety of different fields. - A valuable reference source covering a huge area of materials coverage.


Principles and Applications of Thermal Analysis

Principles and Applications of Thermal Analysis
Author: Paul Gabbott
Publisher: John Wiley & Sons
Total Pages: 480
Release: 2008-04-30
Genre: Science
ISBN: 0470698128

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Thermal Analysis techniques are used in a wide range of disciplines, from pharmacy and foods to polymer science, materials and glasses; in fact any field where changes in sample behaviour are observed under controlled heating or controlled cooling conditions. The wide range of measurements possible provide fundamental information on the material properties of the system under test, so thermal analysis has found increasing use both in basic characterisation of materials and in a wide range of applications in research, development and quality control in industry and academia. Principles and Applications of Thermal Analysis is written by manufacturers and experienced users of thermal techniques. It provides the reader with sound practical instruction on how to use the techniques and gives an up to date account of the principle industrial applications. By covering basic thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) including the new approach of Fast Scanning DSC, together with dynamic mechanical analysis (DMA /TMA) methods, then developing the discussion to encompass industrial applications, the book serves as an ideal introduction to the technology for new users. With a strong focus on practical issues and relating the measurements to the physical behaviour of the materials under test, the book will also serve as an important reference for experienced analysts.


Handbook of Thermal Analysis and Calorimetry

Handbook of Thermal Analysis and Calorimetry
Author: Michael E. Brown
Publisher: Elsevier
Total Pages: 725
Release: 1998-09-07
Genre: Science
ISBN: 0080539599

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Handbook of Thermal Analysis and Calorimetry, Volume 1: Principles and Practice describes the basic background information common to thermal analysis and calorimetry in general. Thermodynamic and kinetic principles are discussed along with the instrumentation and methodology associated with thermoanalytical and calorimetric techniques. The purpose is to collect the discussion of these general principles and minimize redundancies in the subsequent volumes that are concerned with the applications of these principles and methods. More unique methods, which pertain to specific processes or materials, are covered in later volumes.


Theory of Calorimetry

Theory of Calorimetry
Author: W. Zielenkiewicz
Publisher: Springer Science & Business Media
Total Pages: 198
Release: 2006-01-02
Genre: Science
ISBN: 0306484188

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Calorimetry is one of the oldest areas of physical chemistry. The date on which calorimetry came into being may be taken as 13 June 1783, the day on which Lavoisier and Laplace presented a contribution entitled ,,Memoire de la Chaleur“ at a session of the Academie Française. Throughout the existence of calorimetry, many new methods have been developed and the measuring techniques have been improved. At p- sent, numerous laboratories worldwide continue to focus attention on the development and applications of calorimetry, and a number of com- nies specialize in the production of calorimeters. The calorimeter is an instrument that allows heat effects in it to be determined by directly measurement of temperature. Accordingly, to determine a heat effect, it is necessary to establish the relationship - tween the heat effect generated and the quantity measured in the ca- rimeter. It is this relationship that unambiguously determines the mathematical model of the calorimeter. Depending on the type of ca- rimeter applied, the accuracy required, and the conditions of heat and mass transfer that prevail in the device, the relationship between the measured and generated quantities can assume different mathematical forms.