The Valve Actuated Pulse Column Design And Operation PDF Download

A countercurrent extraction column is described which employs timed solenoid valves and pressurized feeds to provide a pulsing action to disperse the phases. The steps in the pulsing cycle are independent and thus provide greater separation of the operating variables than is possible with conventional pulse columns. The column described is particularly useful as a resesrch tool for the study of extraction mechanism although a larger installation operating on the same principles should be quite workable. The 4-stage-cycle or mixersettler type column operation has an inherent advantage in that the rapid coalescence and redispersion of phases are believed to lead to greater extraction than simple movement of a dispersed phase through a continuous medium. In addition, the sharp pulse provided should produce greater turbulence than the more conventional pulsing arrangement. Some results of operation on the extraction and stripping of uranyl nitrate using tributyl phosphate as a solvent are included. These data correspond to Metal Recovery and Erex type systems. (auth).