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Tables of Spectral Data for Structure Determination of Organic Compounds

Tables of Spectral Data for Structure Determination of Organic Compounds
Author: Ernö Pretsch
Publisher: Springer Science & Business Media
Total Pages: 325
Release: 2013-06-29
Genre: Science
ISBN: 3662224550

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Although numerical data are, in principle, universal, the compilations presented in this book are extensively annotated and interleaved with text. This translation of the second German edition has been prepared to facilitate the use of this work, with all its valuable detail, by the large community of English-speaking scientists. Translation has also provided an opportunity to correct and revise the text, and to update the nomenclature. Fortunately, spectroscopic data and their relationship with structure do not change much with time so one can predict that this book will, for a long period of time, continue to be very useful to organic chemists involved in the identification of organic compounds or the elucidation of their structure. Klaus Biemann Cambridge, MA, April 1983 Preface to the First German Edition Making use of the information provided by various spectroscopic tech niques has become a matter of routine for the analytically oriented organic chemist. Those who have graduated recently received extensive training in these techniques as part of the curriculum while their older colleagues learned to use these methods by necessity. One can, therefore, assume that chemists are well versed in the proper choice of the methods suitable for the solution of a particular problem and to translate the experimental data into structural information.


Structural Identification of Organic Compounds with Spectroscopic Techniques

Structural Identification of Organic Compounds with Spectroscopic Techniques
Author: Yong-Cheng Ning
Publisher: Wiley-VCH
Total Pages: 480
Release: 2005-05-06
Genre: Science
ISBN:

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Clearly structured, easy to read and optimal to understand, this extensive compendium fills the gap between textbooks devoted to either spectra interpretation or basic physical principles. The original Chinese editions have already sold over 18,500 copies, and the material is taken from the latest literature from around the world, plus technical information provided by the manufacturers of spectroscopic instruments. Alongside basic methods, Professor Ning presents up-to-date developments in NMR, MS, IR and Raman spectroscopy, such as pulsed-field gradient technique, LC-NMR, and DOSY. He stresses the application of spectroscopic methods, interpreting them in great detail and depth since most of the selected spectra may be applied to practical work, as well as summarizing the rules for their interpretation. He also incorporates his original ideas, including a comparison of the common points in different spectroscopic techniques. This monograph features a unique structure, a typical example being the discussion of 2D NMR starting from pulse sequence units, which construct various pulse sequences for related 2D NMR. A complete chapter deals with the determination of configurations and conformations of organic compounds and even biological molecules from the viewpoint of spectroscopic methodologies, while one whole section is dedicated to the interpretation of mass spectra produced by soft ionization techniques. The principles of mass analyzers, especially the ion trap, are discussed in great depth, together with a concise summary of the MS fragmentation and rearrangement of common compounds, allowing readers to easily predict related mass spectrometric reactions. All the three kinds of library retrieval of mass spectra are presented in detail, together with recent developments in molecular vibration spectroscopy. The whole is rounded off with several appendices, including a subject index for rapid reference. With a foreword by the Nobel prizewinner, Richard R. Ernst.


Structural Identification of Organic Compounds with Spectroscopic Techniques

Structural Identification of Organic Compounds with Spectroscopic Techniques
Author: Yong-Cheng Ning
Publisher: Wiley-VCH
Total Pages: 480
Release: 2005-05-06
Genre: Science
ISBN:

Download Structural Identification of Organic Compounds with Spectroscopic Techniques Book in PDF, ePub and Kindle

Clearly structured, easy to read and optimal to understand, this extensive compendium fills the gap between textbooks devoted to either spectra interpretation or basic physical principles. The original Chinese editions have already sold over 18,500 copies, and the material is taken from the latest literature from around the world, plus technical information provided by the manufacturers of spectroscopic instruments. Alongside basic methods, Professor Ning presents up-to-date developments in NMR, MS, IR and Raman spectroscopy, such as pulsed-field gradient technique, LC-NMR, and DOSY. He stresses the application of spectroscopic methods, interpreting them in great detail and depth since most of the selected spectra may be applied to practical work, as well as summarizing the rules for their interpretation. He also incorporates his original ideas, including a comparison of the common points in different spectroscopic techniques. This monograph features a unique structure, a typical example being the discussion of 2D NMR starting from pulse sequence units, which construct various pulse sequences for related 2D NMR. A complete chapter deals with the determination of configurations and conformations of organic compounds and even biological molecules from the viewpoint of spectroscopic methodologies, while one whole section is dedicated to the interpretation of mass spectra produced by soft ionization techniques. The principles of mass analyzers, especially the ion trap, are discussed in great depth, together with a concise summary of the MS fragmentation and rearrangement of common compounds, allowing readers to easily predict related mass spectrometric reactions. All the three kinds of library retrieval of mass spectra are presented in detail, together with recent developments in molecular vibration spectroscopy. The whole is rounded off with several appendices, including a subject index for rapid reference. With a foreword by the Nobel prizewinner, Richard R. Ernst.


Spectrometric Identification of Organic Compounds

Spectrometric Identification of Organic Compounds
Author: Robert Milton Silverstein
Publisher:
Total Pages: 0
Release: 2005
Genre: Organic compounds
ISBN: 9780471429135

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Originally published in 1962, this was the first book to explore teh identification of organic compounds using spectroscopy. It provides a thorough introduction to the three areas of spectrometry most widely used in spectrometric identification: mass spectrometry, infrared spectrometry, and nuclear magnetic resonance spectrometry. A how-to, hands-on teaching manual with considerably expanded NMR coverage--NMR spectra can now be intrepreted in exquisite detail. This book: Uses a problem-solving approach with extensive reference charts and tables. Offers an extensive set of real-data problems offers a challenge to the practicing chemist


An Introduction to Spectroscopic Methods for the Identification of Organic Compounds

An Introduction to Spectroscopic Methods for the Identification of Organic Compounds
Author: F. Scheinmann
Publisher: Elsevier
Total Pages: 365
Release: 2013-10-22
Genre: Science
ISBN: 1483280837

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An Introduction to Spectroscopic Methods for the Identification of Organic Compounds, Volume 2 covers the theoretical aspects and some applications of certain spectroscopic methods for organic compound identification. This book is composed of 10 chapters, and begins with an introduction to the structure determination from mass spectra. The subsequent chapter presents some mass spectrometry seminar problems and answers. This presentation is followed by discussions on the problems concerning the application of UV spectroscopy and electron spin resonance spectroscopy. Other chapters deal with some advances and development in NMR spectroscopy and the elucidation of structural formula of organic compounds by a combination of spectral methods. The final chapter surveys seminar problems and answers in the identification of organic compounds using NMR, IR, UV and mass spectroscopy. This book will prove useful to organic and analytical chemists.


Structural Analysis of Organic Compounds by Combined Application of Spectroscopic Methods

Structural Analysis of Organic Compounds by Combined Application of Spectroscopic Methods
Author: J.T. Clerc
Publisher: Elsevier
Total Pages: 289
Release: 2012-12-02
Genre: Science
ISBN: 0444597549

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Structural Analysis of Organic Compounds covers some practical analytical aspects of organic structural analysis by combined application of spectroscopic methods. This book is composed of three parts encompassing 35 chapters that specifically describe infrared-, ultraviolet-, proton and carbon-13 nuclear magnetic resonance and mass spectroscopy. Considerable chapters discuss the problems intended to cover a wide variety of chemical structure and spectroscopic argument, thereby exemplifying interpretations and comment on specific practical aspects of the problem solving procedure. The remaining chapters provide short supplementing research concerning various aspects of structural analysis. This book will prove useful to organic and analytical chemists.


Organic Structure Analysis

Organic Structure Analysis
Author: Phillip Crews
Publisher: Oxford University Press, USA
Total Pages: 664
Release: 2010
Genre: Medical
ISBN:

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The most up-to-date integrated spectroscopy text available, Organic Structure Analysis, Second Edition, is the only text that teaches students how to solve structures as they are solved in actual practice. Ideal for advanced undergraduate and graduate courses in organic structure analysis, organic structure identification, and organic spectroscopy, it emphasizes real applications--integrating theory as needed--and introduces students to the latest spectroscopic methods. FEATURES * Focus on Structure: Opens with structural elements and then considers the characteristics, advantages, and disadvantages of spectroscopic methods. Includes coverage of the steps used in determining a molecular structure, the limitations to organic structure determination by spectroscopic methods, and an "Organic Structure Analyses Gone Bad" table (all unique to this text) * Practical Organization: Presents the most commonly used methods first, beginning with an overview of strategies, followed by the use of NMR, and then moving on to mass spectrometry, infrared, and ultraviolet * Innovative Real-World Problem-Solving Approach: Follows the actual information flow used by chemists to solve molecular structures, as opposed to the standard methods-based approach of other texts * Unique Chapter (12) Featuring 51 Structure-Solving Problems: Each problem emphasizes a different method; the problems increase in difficulty throughout the chapter, successively building on students' knowledge and requiring them to integrate multiple methods to identify molecules. NEW TO THE SECOND EDITION * Coverage of the Latest Instrumental and Computational Advances: Examines the use of modern instruments, data processing, and computer-assisted structure elucidation techniques * Updated and Expanded Treatment of NMR (Chapters 2-5): An extensively revised Chapter 5 discusses multi-pulse 1D and 2D NMR methods, 1D TOCSY and 1D NOESY sequences, and using NOESY and ROESY in determining relative stereochemistry and solution conformation. * Additional Coverage of Mass Spectrometry: A new chapter (7) expands the discussion of mass spectrometry to three chapters (6-8). Topics include cutting-edge MS instrumentation and new information on tandem MS techniques, combining NMR with MS, large-molecule MS, chemo-informatics, and more. * More Exercises and Improved Spectra: The second edition includes 25% more problems than the previous edition (279 total). In addition, many of the spectra, including all of those presented in Chapters 11 and 12, have been reprocessed or reacquired for greater clarity.


Organic Structures from Spectra

Organic Structures from Spectra
Author: L. D. Field
Publisher: John Wiley & Sons
Total Pages: 512
Release: 2013-02-18
Genre: Science
ISBN: 1118325451

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The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. A critical part of any such course is a suitable set of problems to develop the student’s understanding of how structures are determined from spectra. Organic Structures from Spectra, Fifth Edition is a carefully chosen set of more than 280 structural problems employing the major modern spectroscopic techniques, a selection of 27 problems using 2D-NMR spectroscopy, more than 20 problems specifically dealing with the interpretation of spin-spin coupling in proton NMR spectra and 8 problems based on the quantitative analysis of mixtures using proton and carbon NMR spectroscopy. All of the problems are graded to develop and consolidate the student’s understanding of organic spectroscopy. The accompanying text is descriptive and only explains the underlying theory at a level which is sufficient to tackle the problems. The text includes condensed tables of characteristic spectral properties covering the frequently encountered functional groups. The examples themselves have been selected to include all important common structural features found in organic compounds and to emphasise connectivity arguments. Many of the compounds were synthesised specifically for this purpose. There are many more easy problems, to build confidence and demonstrate basic principles, than in other collections. The fifth edition of this popular textbook: • includes more than 250 new spectra and more than 25 completely new problems; • now incorporates an expanded suite of new problems dealing with the analysis of 2D NMR spectra (COSY, C H Correlation spectroscopy, HMBC, NOESY and TOCSY); • has been expanded and updated to reflect the new developments in NMR and to retire older techniques that are no longer in common use; • provides a set of problems dealing specifically with the quantitative analysis of mixtures using NMR spectroscopy; • features proton NMR spectra obtained at 200, 400 and 600 MHz and 13C NMR spectra include DEPT experiments as well as proton-coupled experiments; • contains 6 problems in the style of the experimental section of a research paper and two examples of fully worked solutions. Organic Structures from Spectra, Fifth Edition will prove invaluable for students of Chemistry, Pharmacy and Biochemistry taking a first course in Organic Chemistry. Contents Preface Introduction Ultraviolet Spectroscopy Infrared Spectroscopy Mass Spectrometry Nuclear Magnetic Resonance Spectroscopy 2DNMR Problems Index Reviews from earlier editions “Your book is becoming one of the “go to” books for teaching structure determination here in the States. Great work!” “…I would definitely state that this book is the most useful aid to basic organic spectroscopy teaching in existence and I would strongly recommend every instructor in this area to use it either as a source of examples or as a class textbook”. Magnetic Resonance in Chemistry “Over the past year I have trained many students using problems in your book - they initially find it as a task. But after doing 3-4 problems with all their brains activities... working out the rest of the problems become a mania. They get addicted to the problem solving and every time they solve a problem by themselves, their confident level also increases.” “I am teaching the fundamentals of Molecular Spectroscopy and your books represent excellent sources of spectroscopic problems for students.”


Spectroscopic Identification Of Organic Molecules

Spectroscopic Identification Of Organic Molecules
Author: Elnagdi Mohamed Hilmy
Publisher: World Scientific
Total Pages: 204
Release: 2018-10-23
Genre: Science
ISBN: 9813271302

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Researchers in the fields of organic synthesis, pharmaceutical research as well as cosmetic and agrochemicals industries need to confirm the structures of products they obtain. This was previously a time-consuming a process that took up much time. Spectroscopic methods however, made it easier, and initially R and UV helped chemists conclude structures one way or another. Initially 1D NMR, 2D NMR and sophisticated NMR measurements like COESY and NOESY were of great assistance. We demonstrate principles to conclude structures of our simple molecules, mainly heterocycles of interest for researchers in fields indicated above.However, it is insufficient to only understand the principles, and one should also master problem solving and thinking. We demonstrate simple problems like the utility of coupling constants, NOE, COESY and NOESY and show how firm conclusions are obtained in real life. Most NMR books usually demonstrate these principles utilizing a pit sophisticated examples. The methodology suggested by us is simpler and quite useful for researchers in heterocyclic chemistry where combination of proton and carbon NMR should be dealt together.Our research results previously been used intensively (Cf. citations in Google Scholar) and still draw attention. Students in the fields indicated will find this book of value to sign the spectra of the molecules they synthesize. Researchers in the field of heterocyclic chemistry as well as instructors in the field of structure proof utilizing spectroscopic identification will also find this book of interest.