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Principles and Practice of Spectroscopic Calibration

Principles and Practice of Spectroscopic Calibration
Author: Howard Mark
Publisher: John Wiley & Sons
Total Pages: 198
Release: 1992-04-16
Genre: Science
ISBN: 9780471546146

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Dealing with the principles of calibration--both the theoretical and mathematical constructs which relate features of calibration equations to the physical phenomena that affect instruments and samples used on generating information. Among derivations in leading spectroscopic and statistical literature, numerous necessary mathematical derivations have been specifically designed for this book. Covers the practical aspects of generating a calibration equation including how to recognize and deal with various types of problems affecting calibration dataset, relating theoretical ideas, and their affect on data and how to deal with unusual situations.


Principles and Practice of X-Ray Spectrometric Analysis

Principles and Practice of X-Ray Spectrometric Analysis
Author: E.P. Bertin
Publisher: Springer Science & Business Media
Total Pages: 1098
Release: 2012-12-06
Genre: Science
ISBN: 1461344166

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Since the first edition of this book was published early in 1970, three major developments have occurred in the field of x-ray spectrochemical analysis. First, wavelength-dispersive spectrometry, in 1970 already securely established among instrumental analytical methods, has matured. Highly sophisticated, miniaturized, modular, solid-state circuitry has replaced elec tron-tube circuitry in the readout system. Computers are now widely used to program and control fully automated spectrometers and to store, process, and compute analytical concentrations directly and immediately from ac cumulated count data. Matrix effects have largely yielded to mathematical treatment. The problems associated with the ultralong-wavelength region have been largely surmounted. Indirect (association) methods have extended the applicability of x-ray spectrometry to the entire periodic table and even to certain classes of compounds. Modern commercial, computerized, auto matic, simultaneous x-ray spectrometers can index up to 60 specimens in turn into the measurement position and for each collect count data for up to 30 elements and read out the analytical results in 1--4 min-all corrected for absorption-enhancement and particle-size or surface-texture effects and wholly unattended. Sample preparation has long been the time-limiting step in x-ray spectrochemical analysis. Second, energy-dispersive spectrometry, in 1970 only beginning to assume its place among instrumental analytical methods, has undergone phenomenal development and application and, some believe, may supplant wavelength spectrometry for most applications in the foreseeable future.


Spectroscopy

Spectroscopy
Author: Mark F. Vitha
Publisher: John Wiley & Sons
Total Pages: 342
Release: 2018-10-30
Genre: Science
ISBN: 1119436648

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Provides students and practitioners with a comprehensive understanding of the theory of spectroscopy and the design and use of spectrophotometers In this book, you will learn the fundamental principles underpinning molecular spectroscopy and the connections between those principles and the design of spectrophotometers. Spectroscopy, along with chromatography, mass spectrometry, and electrochemistry, is an important and widely-used analytical technique. Applications of spectroscopy include air quality monitoring, compound identification, and the analysis of paintings and culturally important artifacts. This book introduces students to the fundamentals of molecular spectroscopy – including UV-visible, infrared, fluorescence, and Raman spectroscopy – in an approachable and comprehensive way. It goes beyond the basics of the subject and provides a detailed look at the interplay between theory and practice, making it ideal for courses in quantitative analysis, instrumental analysis, and biochemistry, as well as courses focused solely on spectroscopy. It is also a valuable resource for practitioners working in laboratories who regularly perform spectroscopic analyses. Spectroscopy: Principles and Instrumentation: Provides extensive coverage of principles, instrumentation, and applications of molecular spectroscopy Facilitates a modular approach to teaching and learning about chemical instrumentation Helps students visualize the effects that electromagnetic radiation in different regions of the spectrum has on matter Connects the fundamental theory of the effects of electromagnetic radiation on matter to the design and use of spectrophotometers Features numerous figures and diagrams to facilitate learning Includes several worked examples and companion exercises throughout each chapter so that readers can check their understanding Offers numerous problems at the end of each chapter to allow readers to apply what they have learned Includes case studies that illustrate how spectroscopy is used in practice, including analyzing works of art, studying the kinetics of enzymatic reactions, detecting explosives, and determining the DNA sequence of the human genome Complements Chromatography: Principles and Instrumentation The book is divided into five chapters that cover the Fundamentals of Spectroscopy, UV-visible Spectroscopy, Fluorescence/Luminescence Spectroscopy, Infrared Spectroscopy, and Raman Spectroscopy. Each chapter details the theory upon which the specific techniques are based, provides ways for readers to visualize the molecular-level effects of electromagnetic radiation on matter, describes the design and components of spectrophotometers, discusses applications of each type of spectroscopy, and includes case studies that illustrate specific applications of spectroscopy. Each chapter is divided into multiple sections using headings and subheadings, making it easy for readers to work through the book and to find specific information relevant to their interests. Numerous figures, exercises, worked examples, and end-of-chapter problems reinforce important concepts and facilitate learning. Spectroscopy: Principles and Instrumentation is an excellent text that prepares undergraduate students and practitioners to operate in modern laboratories.


Photochemical Vapor Deposition

Photochemical Vapor Deposition
Author: J. G. Eden
Publisher: Wiley-Interscience
Total Pages: 208
Release: 1992-10-07
Genre: Science
ISBN: 9780471550839

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Remote Sensing by Fourier Transform Spectrometry Reinhard Beer Here is a complete introduction to the specification, design, and implementation of Fourier Transform Spectrometers especially intended for atmospheric or astronomical remote sensing. Dr. Beer, one of the pioneers in this field, provides both specific and general information on the development of requirements for remote sensing Fourier transform infrared spectrometers and discusses many of the problems and pitfalls (along with their avoidance and solutions) that can beset the new user. 1992 (0 471-55346-8) 176 pp. Principles and Practice of Spectroscopic Calibration Howard Mark Clearly linking theory with applications, this unique guide to spectroscopic calibration advances an approach that is understandable, free of the usual uncertainties, and simple to execute. The book details the practical aspects of generating a calibration equation, as well as the basics of recognizing and dealing with different types of problems affecting calibration. Most of the procedures are applicable to such sophisticated and popular approaches as Principal Component Calibration, Partial Least Squares Calibration, and Fourier Transform Calibration. 1991 (0 471-54614-3) 192 pp. Activation Spectrometry in Chemical Analysis Susan J. Parry Knowing the specifics of activation analysis has become essential for a wide range of specialists, including chemists, physicists, and biologists, who need to know how to make the most effective use of this technique. In clear, easy-to-read language, this book provides a straightforward review of just what activation analysis can do, describing the technique as it is currently applied to analytical problems. With emphasis on activation spectrometry, Dr. Parry outlines the specifics of the procedure, which, along with other activation analysis methods, have proven critical to the technique's success. 1991 (0 471-63844-7) 264 pp.


Chemometrics in Spectroscopy

Chemometrics in Spectroscopy
Author: Howard Mark
Publisher: Academic Press
Total Pages: 1094
Release: 2021-09-30
Genre: Science
ISBN: 0323911706

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Chemometrics in Spectroscopy, Revised Second Edition provides the reader with the methodology crucial to apply chemometrics to real world data. The book allows scientists using spectroscopic instruments to find explanations and solutions to their problems when they are confronted with unexpected and unexplained results. Unlike other books on these topics, it explains the root causes of the phenomena that lead to these results. While books on NIR spectroscopy sometimes cover basic chemometrics, they do not mention many of the advanced topics this book discusses. This revised second edition has been expanded with 50% more content on advances in the field that have occurred in the last 10 years, including calibration transfer, units of measure in spectroscopy, principal components, clinical data reporting, classical least squares, regression models, spectral transfer, and more. Written in the column format of the authors’ online magazine Presents topical and important chapters for those involved in analysis work, both research and routine Focuses on practical issues in the implementation of chemometrics for NIR Spectroscopy Includes a companion website with 350 additional color figures that illustrate CLS concepts


Handbook of Petroleum Product Analysis

Handbook of Petroleum Product Analysis
Author: James G. Speight
Publisher: John Wiley & Sons
Total Pages: 368
Release: 2015-02-02
Genre: Science
ISBN: 1118986350

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Introduces the reader to the production of the products in a refinery • Introduces the reader to the types of test methods applied to petroleum products, including the need for specifications • Provides detailed explanations for accurately analyzing and characterizing modern petroleum products • Rewritten to include new and evolving test methods • Updates on the evolving test methods and new test methods as well as the various environmental regulations are presented


Handbook of Coal Analysis

Handbook of Coal Analysis
Author: James G. Speight
Publisher: John Wiley & Sons
Total Pages: 367
Release: 2015-03-30
Genre: Science
ISBN: 1118369246

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Provides users with everything they need to know about testing and analysis of coal Includes new coverage on environmental issues and regulations as related to coal Provides the reader with the necessary information about testing and analyzing coal and relays the advantages and limitations in understanding the quality and performance of coal Explains the meaning of test results and how these results can predict coal behavior and its corresponding environmental impact during use Includes a comprehensive Glossary which defines items in straightforward language that enable readers to better understand the terminology related to coal Treats issues related to sampling, and accuracy and precision of analysis


Circulating Tumor Cells

Circulating Tumor Cells
Author: Z. Hugh Fan
Publisher: John Wiley & Sons
Total Pages: 505
Release: 2016-03-25
Genre: Science
ISBN: 1119244544

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Introduces the reader to Circulating Tumor Cells (CTCs), their isolation method and analysis, and commercially available platforms Presents the historical perspective and the overview of the field of circulating tumor cells (CTCs) Discusses the state-of-art methods for CTC isolation, ranging from the macro- to micro-scale, from positive concentration to negative depletion, and from biological-property-enabled to physical-property-based approaches Details commercially available CTC platforms Describes post-isolation analysis and clinical translation Provides a glossary of scientific terms related to CTCs


Hydrophilic Interaction Chromatography

Hydrophilic Interaction Chromatography
Author: Bernard A. Olsen
Publisher: John Wiley & Sons
Total Pages: 336
Release: 2013-01-22
Genre: Science
ISBN: 1118054172

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Discover how to use HILIC to analyze and better understand polar compounds An increasingly popular analytical method, hydrophilic interaction chromatography (HILIC) has the ability to retain and separate polar compounds that are often difficult to analyze by reversed-phase high-performance liquid chromatography (HPLC) or other analytical methods. Offering a comprehensive review, this book enables readers to develop a fundamental understanding of how HILIC works and then apply that knowledge to develop and implement a variety of practical applications. Hydrophilic Interaction Chromatography begins with discussions of HILIC retention mechanisms, stationary phases, and general method development. This sets the foundation for the book's extensive coverage of applications. The authors address unique separation challenges for bioanalytical, environmental, pharmaceutical, and biochemical applications. Moreover, there is a thorough discussion of HILIC in two-dimensional chromatography. With contributions from leading analytical scientists who have extensive experience in HILIC as well as HPLC, Hydrophilic Interaction Chromatography serves as a practical guide for researchers, featuring: Detailed examples of HILIC methods and development approaches Thorough explanations of retention mechanisms and the impact of stationary phase and mobile phase properties on separations Step-by-step guidance for developing efficient, sensitive, and robust HILIC methods References to the primary literature at the end of each chapter Hydrophilic Interaction Chromatography is written for scientists who use or develop analytical methods for the separation of polar compounds. In particular, these researchers will discover how HILIC can be used to analyze and better understand the composition of pharmaceutical, bioanalytical, biochemical, chemical, food, and environmental samples.


Process Analytical Technology

Process Analytical Technology
Author: Katherine A. Bakeev
Publisher: John Wiley & Sons
Total Pages: 576
Release: 2010-04-01
Genre: Science
ISBN: 0470689609

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Process Analytical Technology explores the concepts of PAT and its application in the chemical and pharmaceutical industry from the point of view of the analytical chemist. In this new edition all of the original chapters have been updated and revised, and new chapters covering the important topics of sampling, NMR, fluorescence, and acoustic chemometrics have been added. Coverage includes: Implementation of Process Analytical Technologies UV-Visible Spectroscopy for On-line Analysis Infrared Spectroscopy for Process Analytical Applications Process Raman Spectroscopy Process NMR Spectrscopy: Technology and On-line Applications Fluorescent Sensing and Process Analytical Applications Chemometrics in Process Analytical Technology (PAT) On-Line PAT Applications of Spectroscopy in the Pharmaceutical Industry Future Trends for PAT for Increased Process Understanding and Growing Applications in Biomanufacturing NIR Chemical Imaging This volume is an important starting point for anyone wanting to implement PAT and is intended not only to assist a newcomer to the field but also to provide up-to-date information for those who practice process analytical chemistry and PAT. It is relevant for chemists, chemical and process engineers, and analytical chemists working on process development, scale-up and production in the pharmaceutical, fine and specialty chemicals industries, as well as for academic chemistry, chemical engineering, chemometrics and pharmaceutical science research groups focussing on PAT. Review from the First Edition “The book provides an excellent first port of call for anyone seeking material and discussions to understand the area better. It deserves to be found in every library that serves those who are active in the field of Process Analytical Technology.”—Current Engineering Practice