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Practical NMR Spectroscopy Laboratory Guide: Using Bruker Spectrometers

Practical NMR Spectroscopy Laboratory Guide: Using Bruker Spectrometers
Author: John S. Harwood
Publisher: Academic Press
Total Pages: 137
Release: 2015-10-28
Genre: Science
ISBN: 0128007192

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Practical NMR Spectroscopy Laboratory Guide is designed to provide non-expert NMR users, typically graduate students in chemistry, an introduction to various facets of practical solution-state NMR spectroscopy. Each chapter offers a series of hands-on exercises, introducing various NMR concepts and experiments and guiding the reader in running these experiments using an NMR spectrometer. The book is written for use with a Bruker NMR spectrometer running TopSpin software versions 1 or 2. This practical resource functions both as a text for instructors of a practical NMR course and also as a reference for spectrometer administrators or NMR facility directors when doing user training. This guide serves as serve as excellent, practical resource on its own or as a companion book to Timothy Claridge’s High-Resolution NMR Techniques in Organic Chemistry, 2nd Edition (Elsevier, 2009). Written by experts in solution-state NMR spectroscopy Provides step-by-step instructions for more than 50 activities using a Bruker NMR spectrometer Includes detailed appendices and sample questions for lab reports


Handbook of Spectroscopy

Handbook of Spectroscopy
Author: G¿nter Gauglitz
Publisher: John Wiley & Sons
Total Pages: 1168
Release: 2006-03-06
Genre: Science
ISBN: 3527605029

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This handbook provides a straightforward introduction to spectroscopy, showing what it can do and how it does it, together with a clear, integrated and objective account of the wealth of information that can be derived from spectra. The sequence of chapters covers a wide range of the electromagnetic spectrum, and the physical processes involved, from nuclear phenomena to molecular rotation processes. - A day-by-day laboratory guide: its design based on practical knowledge of spectroscopists at universities, industries and research institutes - A well-structured information source containing methods and applications sections framed by sections on general topics - Guides users to a decision about which spectroscopic method and which instrumentation will be the most appropriate to solve their own practical problem - Rapid access to essential information - Correct analysis of a huge number of measured spectra data and smart use of such information sources as databases and spectra libraries


50 and More Essential NMR Experiments

50 and More Essential NMR Experiments
Author: Matthias Findeisen
Publisher: John Wiley & Sons
Total Pages: 322
Release: 2013-11-04
Genre: Science
ISBN: 3527334831

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This book is the perfect link for learning how to perform the experiments after only having studied theory. In eight chapters more than 50 essential NMR experiments are described in detail. Special focus is put on the organic set of NMR spectra (1H, 13C-APT, COSY, NOESY, HSQC and HMBC). Different chapters deal with advanced organic NMR, selective methods, heteronuclear NMR, relaxation and diffusion measurements, organic applications and maintenance. Every experiment has a section providing the reader with the purpose and scope of the specific experiment. Every experiment is concluded with the spectrum as it is obtained under the conditions described. Questions and comments enable the reader to check their understanding. The authors are very experienced and the whole book is in full color, which enhances the reading experience and makes the spectra and other figures easier to understand. This book is strongly recommended for all students and researchers who are involved in the structural elucidation of chemical compounds both in practical education and in pursuing research, in particular if they handle an NMR spectrometer.


NMR-Spectroscopy: Data Acquisition

NMR-Spectroscopy: Data Acquisition
Author: Christian Schorn
Publisher: John Wiley & Sons
Total Pages: 392
Release: 2004-09-03
Genre: Science
ISBN: 9783527310708

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This volume enables the newcomer to become familiar with the basic data acquisition procedures, modular pulse sequence units and complete sequences in NMR spectroscopy.


Practical NMR Spectroscopy

Practical NMR Spectroscopy
Author: Maryvonne L. Martin
Publisher:
Total Pages: 460
Release: 1980
Genre: Nuclear magnetic resonance
ISBN: 9780855014629

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Hands on NMR

Hands on NMR
Author: William S. Price
Publisher:
Total Pages: 500
Release: 2021-05-17
Genre: Science
ISBN: 9781788010887

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Presenting important practical aspects of NMR spectroscopy, this book will be useful for explaining and facilitating the successful set up of a wide variety of NMR experiments. It will enlighten readers with the relevant information on the basic concepts in NMR, how it works, and how to trouble-shoot artefacts that may be encountered. A short introductory chapter on some basic theory and key concepts will precede chapters on more practical aspects e.g. instrumentation, sample preparation, experimentation and data processing. Several practical case experiments covering various fields and including details on the pitfalls, tips and recommendations are presented next. Lastly, detailed chapters on other important practical aspects such as artefacts, spectral prediction, databases and safety are included. Bringing books that present practical NMR up to date, this book fills a gap in the literature and provides a new comprehensive practical NMR book for teaching and research at all levels - graduates, postgraduates, industry and research.


Essential Practical NMR for Organic Chemistry

Essential Practical NMR for Organic Chemistry
Author: S. A. Richards
Publisher: John Wiley & Sons
Total Pages: 293
Release: 2023-05-01
Genre: Science
ISBN: 1119844800

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A hands-on resource advocating an ordered approach to gathering and interpreting NMR data The second edition of Essential Practical NMR for Organic Chemistry delivers a pragmatic and accessible text demonstrating an ordered approach to gathering and interpreting NMR data. In this informal guide, you’ll learn to make sense of the high density of NMR information through the authors’ problem-solving strategies and interpretations. The book also discusses critical aspects of NMR theory, as well as data acquisition and processing strategy. It explains the use of NMR spectroscopy for dealing with problems of small organic molecule structural elucidation and includes a brand-new chapter on Nitrogen-15 NMR. Readers will also find: Strategies for preparing a sample, spectrum acquisition, processing, and interpreting your spectrum Fulsome discussions of Carbon-13 NMR spectroscopy Practical treatments of quantification, safety procedures, and relevant software An ideal handbook for anyone involved in using NMR to solve structural problems, this latest edition of Essential Practical NMR for Organic Chemistry will be particularly useful for chemists running and looking at their own NMR spectra, as well as those who work in small molecule NMR. It will also earn a place in the libraries of undergraduate and post-graduate organic chemistry students.


NMR-Spectroscopy: Data Acquisition

NMR-Spectroscopy: Data Acquisition
Author: Christian Schorn
Publisher: John Wiley & Sons
Total Pages: 376
Release: 2001
Genre: Science
ISBN: 9783527288274

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The key to correct structure analysis. This volume of the successful "Spectroscopic Techniques" series familiarizes newcomers with the basic data acquisition procedures, modular pulse sequence units and complete sequences in NMR spectroscopy. It applies the numerous possibilities of Bruker's simulation program NMR-SIM to provide a guided introduction to the world of pulse sequences. The effectiveness of particular NMR experiments is demonstrated by the section "Check Its" and that of data processing by the accompanying CD-ROM with the Bruker processing software 1D and 2D WIN-NMR. This interactive approach to simulate spectra based on a reduced spin system and the processing of the accomplished NMR raw data is closely related to everyday work at the spectrometer. In this way, the author encourages beginners to use high resolution NMR, and also experts on NMR spectroscopy to evaluate new experiments using the easy-manageable simulation program.


NMR Spectroscopy Techniques, Second Edition,

NMR Spectroscopy Techniques, Second Edition,
Author: Martha Bruch
Publisher: CRC Press
Total Pages: 634
Release: 1996-03-05
Genre: Science
ISBN: 9780585374901

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This work elucidates the power of modern nuclear magnetic resonance (NMR) techniques to solve a wide range of practical problems that arise in both academic and industrial settings. This edition provides current information regarding the implementation and interpretation of NMR experiments, and contains material on: three- and four-dimensional NMR; the NMR analysis of peptides, proteins, carbohydrates and oligonucleotides; and more.


Practical NMR Spectroscopy

Practical NMR Spectroscopy
Author: Maryvonne L. Martin
Publisher:
Total Pages: 460
Release: 1980
Genre:
ISBN: 9780317263268

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