Nmr Spectroscopy Of The Non Metallic Elements PDF Download
Are you looking for read ebook online? Search for your book and save it on your Kindle device, PC, phones or tablets. Download Nmr Spectroscopy Of The Non Metallic Elements PDF full book. Access full book title Nmr Spectroscopy Of The Non Metallic Elements.
| Author | : Stefan Berger |
| Publisher | : John Wiley & Sons |
| Total Pages | : 1114 |
| Release | : 1997-08-04 |
| Genre | : Science |
| ISBN | : |
Download NMR Spectroscopy of the Non-Metallic Elements Book in PDF, ePub and Kindle
NMR Spectroscopy of the Non-Metallic Elements Stefan Berger Philipps-Universität, Marburg, Germany Siegmar Braun Technische Hochschule Darmstadt, Germany Hans-Otto Kalinowski Justus-Liebig-Universität, Gießen, Germany In recent years, the technique of Nuclear Magnetic Resonance (NMR) Spectroscopy has rapidly gained in importance outside its traditional areas of proton NMR and carbon-13 NMR. In particular, it has become much more applicable to compounds containing elements such as phosphorus, nitrogen and fluorine. NMR Spectroscopy of the Non-Metallic Elements gathers together a wealth of NMR data for the most important non-metallic elements, namely nitrogen, oxygen, fluorine, phosphorus, sulphur and xenon. For each element, the data for the simpler compounds and their derivatives (both organic and inorganic) are gathered together in as complete a form as possible, and the regularities that emerge are discussed in detail in relation to structural variations. This allows the reader to interpret the structure of more complex structures. The chapters containing the NMR data for the elements are preceded by a practical introduction to the basic theory and experimental techniques of the NMR parameters, especially the chemical shift and indirect spin-spin coupling. This material will help the reader both in finding practical solutions to problems of structure determination, and in critically evaluating the spectra obtained. NMR Spectroscopy of the Non-Metallic Elements is an invaluable reference source for all laboratories where NMR is used. It will also be widely used by organic and inorganic chemists, especially those working on nitrogen, fluorine and phosphorus compounds.
| Author | : E. Sherwin |
| Publisher | : Elsevier |
| Total Pages | : 201 |
| Release | : 2016-05-13 |
| Genre | : Science |
| ISBN | : 1483139050 |
Download Chemistry of the Non-Metallic Elements Book in PDF, ePub and Kindle
Chemistry of the Non-Metallic Elements is concerned with the non-metals and is to be read in conjunction with The Chemistry of the Metallic Elements by D. M. McC. Steele. The object has not been to provide an encyclopedic coverage of all the chemical reactions of non-metals but rather to select those which will enable the student to appreciate better the similarities and differences between the elements. The book discusses the chemistry of the non-metals in relation to their positions in the periodic groups. It covers the noble gases, hydrogen, the halogens, Group VIB, oxygen, sulfur, Group VB, nitrogen, phosphorus, carbon, and silicon. Where the groups contain metals, as in Group IVA, their chemistry is briefly discussed to show the properties which occur. This book provides a comprehensive treatment of chemistry at the intermediate level, that is, the sixth-form/first-year university level. Readers are assumed to have a background of O-level chemistry and of O- or A-level physics and a working knowledge of elementary mathematics.
| Author | : Horst Friebolin |
| Publisher | : John Wiley & Sons |
| Total Pages | : 452 |
| Release | : 2010-12-28 |
| Genre | : Science |
| ISBN | : 3527327827 |
Download Basic One- and Two-Dimensional NMR Spectroscopy Book in PDF, ePub and Kindle
This is the fifth edition of the highly successful, classic textbook for bachelor and master courses, with over 20 % new material and the contents completely revised and updated. Using a minimum of mathematics, it explains the underlying theory of this most important spectroscopic technique in a thorough, yet readily understandable way, covering instrumentation and interpretation of the spectra. It presents all students need to know about 1D, 2D-NMR, solid state and dynamic NMR spectroscopy, as well as NMR imaging, all illustrated by examples for maximum clarity. All the sections include sub-chapters that focus on applications taken from organic, macromolecular, polymer and biochemistry. A must for students and lecturers in chemistry, biochemistry, pharmacy, and life sciences, as well as for spectroscopists.
| Author | : J.W. Akitt |
| Publisher | : CRC Press |
| Total Pages | : 422 |
| Release | : 2017-12-21 |
| Genre | : Science |
| ISBN | : 1351991124 |
Download NMR and Chemistry Book in PDF, ePub and Kindle
Keeping mathematics to a minimum, this book introduces nuclear properties, nuclear screening, chemical shift, spin-spin coupling, and relaxation. It is one of the few books that provides the student with the physical background to NMR spectroscopy from the point of view of the whole of the periodic table rather than concentrating on the narrow applications of 1H and 13C NMR spectroscopy. Aids to structure determination, such as decoupling, the nuclear Overhauser effect, INEPT, DEPT, and special editing, and two dimensional NMR spectroscopy are discussed in detail with examples, including the complete assignment of the 1H and 13C NMR spectra of D-amygdain. The authors examine the requirements of a modern spectrometer and the effects of pulses and discuss the effects of dynamic processes as a function of temperature or pressure on NMR spectra. The book concludes with chapters on some of the applications of NMR spectroscopy to medical and non-medical imaging techniques and solid state chemistry of both I = F1/2 and I > F1/2 nuclei. Examples and problems, mainly from the recent inorganic/organometallic chemistry literature support the text throughout. Brief answers to all the problems are provided in the text with full answers at the end of the book.
| Author | : Ursula Weber |
| Publisher | : John Wiley & Sons |
| Total Pages | : 409 |
| Release | : 2008-11-21 |
| Genre | : Science |
| ISBN | : 3527612327 |
Download NMR-Spectroscopy: Modern Spectral Analysis Book in PDF, ePub and Kindle
The state-of-the-art in NMR spectral analysis. This interactive tutorial provides readers with a comprehensive range of software tools and techniques, as well as the necessary theoretical knowledge required to analyze their spectra and obtain the correct NMR parameters. Modern Spectral Analysis provides expert guidance, by presenting efficient strategies to extract NMR parameters from measured spectra. A database of selected spectra and modern, powerful WIN-NMR software designed by Bruker are provided on the enclosed CD-ROM. The programs provided are 1 D WIN-NMR, WIN-DAISY, WIN-DR and WIN-DYNAMICS, and direct data exchange between all these programs is possible. Readers are shown how they can obtain maximum structural information from their 1 D NMR spectra with time-saving computer assistance. Practical problems that can occur and their solutions are discussed at length using clear, easy-to-follow examples. Both homo- and heteronuclear and first- and second-order spin systems are demonstrated. Moreover, relaxation analysis, nuclear Overhauser effects and magnetic site exchange are all covered in this hands-on guide to NMR spectral analysis.
| Author | : G Davidson |
| Publisher | : Royal Society of Chemistry |
| Total Pages | : 474 |
| Release | : 2007-10-31 |
| Genre | : Science |
| ISBN | : 1847555152 |
Download Spectroscopic Properties of Inorganic and Organometallic Compounds Book in PDF, ePub and Kindle
Spectroscopic Properties of Inorganic and Organometallic Compounds provides a unique source of information on an important area of chemistry. Divided into sections mainly according to the particular spectroscopic technique used, coverage in each volume includes: NMR (with reference to stereochemistry, dynamic systems, paramagnetic complexes, solid state NMR and Groups 13-18); nuclear quadrupole resonance spectroscopy; vibrational spectroscopy of main group and transition element compounds and coordinated ligands; and electron diffraction. Reflecting the growing volume of published work in this field, researchers will find this Specialist Periodical Report an invaluable source of information on current methods and applications. Specialist Periodical Reports provide systematic and detailed review coverage in major areas of chemical research. Compiled by teams of leading experts in their specialist fields, this series is designed to help the chemistry community keep current with the latest developments in their field. Each volume in the series is published either annually or biennially and is a superb reference point for researchers. www.rsc.org/spr
| Author | : Iwona Wawer |
| Publisher | : Elsevier |
| Total Pages | : 525 |
| Release | : 2017-07-07 |
| Genre | : Science |
| ISBN | : 008095152X |
Download NMR Spectroscopy in Pharmaceutical Analysis Book in PDF, ePub and Kindle
For almost a decade, quantitative NMR spectroscopy (qNMR) has been established as valuable tool in drug analysis. In all disciplines, i. e. drug identification, impurity profiling and assay, qNMR can be utilized. Separation techniques such as high performance liquid chromatography, gas chromatography, super fluid chromatography and capillary electrophoresis techniques, govern the purity evaluation of drugs. However, these techniques are not always able to solve the analytical problems often resulting in insufficient methods. Nevertheless such methods find their way into international pharmacopoeias. Thus, the aim of the book is to describe the possibilities of qNMR in pharmaceutical analysis. Beside the introduction to the physical fundamentals and techniques the principles of the application in drug analysis are described: quality evaluation of drugs, polymer characterization, natural products and corresponding reference compounds, metabolism, and solid phase NMR spectroscopy for the characterization drug substances, e.g. the water content, polymorphism, and drug formulations, e.g. tablets, powders. This part is accompanied by more special chapters dealing with representative examples. They give more detailed information by means of concrete examples. Combines theory, techniques, and concrete applications—all of which closely resemble the laboratory experience Considers international pharmacopoeias, addressing the concern for licensing Features the work of academics and researchers, appealing to a broad readership
| Author | : Antony Williams |
| Publisher | : Royal Society of Chemistry |
| Total Pages | : 532 |
| Release | : 2016-12-14 |
| Genre | : Science |
| ISBN | : 1849733937 |
Download Modern NMR Approaches to the Structure Elucidation of Natural Products Book in PDF, ePub and Kindle
The Ghanian plant Cryptolepis sanguinolenta is the source of a series of fascinating indoloquinoline alkaloids. The most unusual member of this alkaloid series was initially proposed to be a spiro nonacyclic structure, named cryptospirolepine, and was elucidated in 1993 based on the technologies available at that time. There were, however, several annoying attributes to the structure that bothered analysts for the ensuing 22 years. During the two decades that followed the initial work there have been enormous developments in NMR technology. Using new experimental approaches, specifically homodecoupled 1,1- and 1,n-HD-ADEQUATE NMR experiments developed in 2014, the structure of only a 700 µg sample of cryptospirolepine has been revised and is shown on the cover of this volume. The confluence of the NMR technological and methodological advances that allowed the revision of the structure of cryptospirolepine using a submilligram sample seems a fitting example for this book, which is dedicated to the NMR characterization of various classes of natural products. Volume 2 considers data processing and algorithmic based analyses tailored to natural product structure elucidation and reviews the application of NMR to the analysis of a series of different natural product families including marine natural products, terpenes, steroids, alkaloids and carbohydrates. Volume 1 discusses contemporary NMR approaches including optimized and future hardware and experimental approaches to obtain both the highest quality and most appropriate spectral data for analysis. These books, bringing together acknowledged experts, uniquely focus on the combination of experimental approaches and modern hardware and software applied to the structure elucidation of natural products. The volumes will be an essential resource for NMR spectroscopists, natural product chemists and industrial researchers working on natural product analysis or the characterization of impurities and degradation products of pharmaceuticals that can be as scarce as natural product samples.
| Author | : Oliver Zerbe |
| Publisher | : John Wiley & Sons |
| Total Pages | : 581 |
| Release | : 2013-11-26 |
| Genre | : Science |
| ISBN | : 3527677836 |
Download Applied NMR Spectroscopy for Chemists and Life Scientists Book in PDF, ePub and Kindle
From complex structure elucidation to biomolecular interactions - this applicationoriented textbook covers both theory and practice of modern NMR applications. Part one sets the stage with a general description of NMR introducing important parameters such as the chemical shift and scalar or dipolar couplings. Part two describes the theory behind NMR, providing a profound understanding of the involved spin physics, deliberately kept shorter than in other NMR textbooks, and without a rigorous mathematical treatment of all the physico-chemical computations. Part three discusses technical and practical aspects of how to use NMR. Important phenomena such as relaxation, exchange, or the nuclear Overhauser effects and the methods of modern NMR spectroscopy including multidimensional experiments, solid state NMR, and the measurement of molecular interactions are the subject of part four. The final part explains the use of NMR for the structure determination of selected classes of complex biomolecules, from steroids to peptides or proteins, nucleic acids, and carbohydrates. For chemists as well as users of NMR technology in the biological sciences.
| Author | : Graham A. Webb |
| Publisher | : Elsevier |
| Total Pages | : 288 |
| Release | : 2006-03-15 |
| Genre | : Science |
| ISBN | : 0080461972 |
Download Annual Reports on NMR Spectroscopy Book in PDF, ePub and Kindle
Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has grown to such importance as NMR spectroscopy. It is used in all branches of science where precise structural determination is required and where the nature of interactions and reactions in solution is being studied. Annual Reports on NMR has established itself as a premier means for the specialist and nonspecialist alike to become familiar with new techniques and applications of NMR spectroscopy. * Includes comprehensive review articles on NMR Spectroscopy* Provides nonspecialists using this technology in all branches of science with the latest developments in the field* Keeps specialists up-to-date on the newest techniques in this important and fast-changing field
