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Nanoscale Liquid Interfaces

Nanoscale Liquid Interfaces
Author: Thierry Ondarçuhu
Publisher: CRC Press
Total Pages: 782
Release: 2013-04-17
Genre: Science
ISBN: 9814316458
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This book addresses the recent developments in the investigation and manipulation of liquids at the nanoscale. This new field has shown important breakthroughs on the basic understanding of physical mechanisms involving liquid interfaces, which led to applications in nanopatterning. It has also consequences in force microscopy imaging in liquid environment. The book proposes is a timely review of these various aspects. It is co-authored by 25 among the most prominent scientists in the field.

Nanoscale Probes of the Solid/Liquid Interface

Nanoscale Probes of the Solid/Liquid Interface
Author: Andrew A. Gewirth
Publisher: Springer Science & Business Media
Total Pages: 340
Release: 2013-04-17
Genre: Science
ISBN: 9401584354
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Nanoscale Probes of the Solid--Liquid Interface deals with the use of the scanning tunnelling microscope (STM) and related instrumentation to examine the phenomena occurring at the interface between solid and liquid. Scanning probe microscopy (the collective term for such instruments as the STM, the atomic force microscope and related instrumentation) allows detailed, real space atomic or lattice scale insight into surface structures, information which is ideally correlated with surface reactivity. The use of SPM methods is not restricted to ultrahigh vacuum: the STM and AFM have been used on samples immersed in solution or in ambient air, thus permitting a study of environmental effects on surfaces. At the solid--liquid interface the reactivity derives precisely from the presence of the solution and, in many cases, the application of an external potential. Topics covered in the present volume include: the advantages of studying the solid--liquid interface and the obtaining of additional information from probe measurements; interrelationships between probe tip, the interface and the tunnelling process; STM measurements on semiconductor surfaces; the scanning electrochemical microscope, AFM and the solid--liquid interface; surface X-ray scattering; cluster formation on graphite electrodes; Cu deposition on Au surfaces; macroscopic events following Cu deposition; deposition of small metallic clusters on carbon; overpotential deposition of metals; underpotential deposition; STM on nanoscale ceramic superlattices; reconstruction events on Au(ijk) surfaces; Au surface reconstructions; friction force measurements on graphite steps under potential control; and the biocompatibility of materials.

Assemblies of Gold Nanoparticles at Liquid-Liquid Interfaces

Assemblies of Gold Nanoparticles at Liquid-Liquid Interfaces
Author: Evgeny Smirnov
Publisher: Springer
Total Pages: 258
Release: 2018-04-19
Genre: Technology & Engineering
ISBN: 3319779141
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This book is devoted to various aspects of self-assembly of gold nanoparticles at liquid-liquid interfaces and investigation of their properties. It covers primarily two large fields: (i) self-assembly of nanoparticles and optical properties of these assemblies; and (ii) the role of nanoparticles in redox electrocatalysis at liquid-liquid interfaces. The first part aroused from a long-lasting idea to manipulate adsorption of nanoparticles at liquid-liquid with an external electric field to form 'smart' mirrors and/or filters. Therefore, Chapters 3 to 5 are dedicated to explore fundamental aspects of charged nanoparticles self-assembly and to investigate optical properties (extinction and reflectance) in a through manner. Novel tetrathiafulvalene (TTF)-assisted method leads to self-assembly of nanoparticles into cm-scale nanofilms or, so-called, metal liquid-like droplets (MeLLDs) with remarkable optical properties. The second part (Chapters 6 to 8) clarifies the role of nanoparticles in interfacial electron transfer reactions. They demonstrate how nanoparticles are charged and discharged upon equilibration of Fermi levels with redox couples in solution and how it can be used to perform HER and ORR. Finally, Chapter 9 gives a perspective outlook, including applications of suggested methods in fast, one-step preparation of colloidosomes, SERS substrates as well as pioneer studies on so-called Marangony-type shutters drive by the electric field.

Nanoscale Characterization of Surfaces and Interfaces

Nanoscale Characterization of Surfaces and Interfaces
Author: N. John DiNardo
Publisher: John Wiley & Sons
Total Pages: 173
Release: 2008-09-26
Genre: Technology & Engineering
ISBN: 3527615946
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Derived from the highly acclaimed series Materials Science and Technology, this book provides in-depth coverage of STM, AFM, and related non-contact nanoscale probes along with detailed applications, such as the manipulation of atoms and clusters on a nanometer scale. The methods are described in terms of the physics and the technology of the methods and many high-quality images demonstrate the power of these techniques in the investigation of surfaces and the processes which occur on them. Topics include: Semiconductor Surfaces and Interfaces * Insulators * Layered Compounds * Charge Density Wave Systems * Superconductors * Electrochemisty at Liquid-Solid Interfaces * Biological Systems * Metrological Applications * Nanoscale Surface Forces * Nanotribology * Manipulation on the Nanoscale Materials scientists, surface scientists, electrochemists, as well as scientists working in catalysis and microelectronics will find this book an invaluable source of information

Nanoscale Electrochemistry

Nanoscale Electrochemistry
Author: Andrew J. Wain
Publisher: Elsevier
Total Pages: 580
Release: 2021-09-14
Genre: Technology & Engineering
ISBN: 0128200561
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Nanoscale Electrochemistry focuses on challenges and advances in electrochemical nanoscience at solid–liquid interfaces, highlighting the most prominent developments of the last decade. Nanotechnology has had a tremendous effect on the multidisciplinary field of electrochemistry, yielding new fundamental insights that have broadened our understanding of interfacial processes and stimulating new and diverse applications. The book begins with a tutorial chapter to introduce the principles of nanoscale electrochemical systems and emphasize their unique behavior compared with their macro/microscopic counterparts. Building on this, the following three chapters present analytical applications, such as sensing and electrochemical imaging, that are familiar to the traditional electrochemist but whose extension to the nanoscale is nontrivial and reveals new chemical information. The subsequent three chapters present exciting new electrochemical methodologies that are specific to the nanoscale, including "single entity"-based methods and surface-enhanced electrochemical spectroscopy. These techniques, now sufficiently mature for exposition, have paved the way for major developments in our understanding of solid–liquid interfaces and continue to push electrochemical analysis toward atomic-length scales. The final three chapters address the rich overlap between electrochemistry and nanomaterials science, highlighting notable applications in energy conversion and storage. This is an important reference for both academic and industrial researchers who are seeking to learn more about how nanoscale electrochemistry has developed in recent years. Outlines the major applications of nanoscale electrochemistry in energy storage, spectroscopy and biology Summarizes the major principles of nanoscale electrochemical systems, exploring how they differ from similar system types Discusses the major challenges of electrochemical analysis at the nanoscale

Liquid Surfaces and Interfaces

Liquid Surfaces and Interfaces
Author: Peter S. Pershan
Publisher: Cambridge University Press
Total Pages: 335
Release: 2012-08-02
Genre: Science
ISBN: 0521814014
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A practical guide for graduate students and researchers on all aspects of x-ray scattering experiments on liquid surfaces and interfaces.

Generation of Polymers and Nanomaterials at Liquid-Liquid Interfaces

Generation of Polymers and Nanomaterials at Liquid-Liquid Interfaces
Author: Panagiotis Dallas
Publisher: Elsevier
Total Pages: 226
Release: 2020-07-28
Genre: Science
ISBN: 0128195053
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Generation of Polymers and Nanomaterials at Liquid-Liquid Interfaces: Application to Crystalline, Light Emitting, and Energy Materials, Second Edition is an innovative guide to the synthesis and processing of materials through liquid-liquid interfaces. This second edition has been revised and expanded, with a new chapter on light emitting materials and increased emphasis towards applications. The book aims to highlight the versatility of the interface between two liquids, providing a unique environment for synthesizing materials with highly tuned, desirable properties. In this revised and expanded second edition, the advanced applications of the synthesized materials and the two-phase systems are highlighted, with real potential within flexible electronics, energy storage, enhanced oil recovery, and sensors. This is supported by detailed coverage of interfacial processes and the fundamental physical chemistry behind them. The first two chapters provide an overview of interfaces in natural and biological systems, and outline the fundamental properties of the interface. Chapters 3 and 4 are devoted to the synthesis and self-organization of nanoparticles and polymers through interfacial systems. The synthesis of conductive, fluorescent and conventional polymers and their properties are extensively covered. Chapters 5 and 6 focus on novel applications. This book is of interest to researchers, scientists, and advanced students, in polymer synthesis, polymer chemistry, polymer science, nanomaterials and nanotechnology, polymer composites, materials science, energy, flexible electronics, and chemical engineering. In industry, this supports scientists, R&D, and other professionals, working with polymeric materials for applications in energy, electronics, sensors, and oil & gas. Provides new ideas for the design of fluorescent polymers, conductive polymers, nanoparticle arrays, thin films, and novel 2D materials Includes detailed coverage of synthesis and processing of polymers and nanomaterials at liquid-liquid interfaces Explores state-of-the-art applications across flexible electronics, energy storage, enhanced oil recovery, and sensors