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Miniaturization in Sample Preparation

Miniaturization in Sample Preparation
Author: Francisco Pena Pereira
Publisher: Walter de Gruyter GmbH & Co KG
Total Pages: 464
Release: 2014-12-02
Genre: Science
ISBN: 3110410184

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Miniaturization is a challenge thrown down to analytical chemistry. The replacement of conventional analytical systems by miniaturized alternatives during the last years is noticeable. Specifically, the miniaturization of traditional sample preparation techniques (e.g., solid-phase extraction or solvent extraction) led to the development of environmentally benign analytical methods. This book aims to provide an overview of the challenges and achievements inthe application of the miniaturized sample preparation methods in analytical laboratories. It includes both theoretical and practical aspects of miniaturized sample preparation approaches and hence should be of interest to researchers, students and teachers of analytical and bioanalytical chemistry, environmental sciences and environmental engineering.


Handbook on Miniaturization in Analytical Chemistry

Handbook on Miniaturization in Analytical Chemistry
Author: Chaudhery Mustansar Hussain
Publisher: Elsevier
Total Pages: 368
Release: 2020-07-25
Genre: Science
ISBN: 012822553X

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Handbook on Miniaturization in Analytical Chemistry: Application of Nanotechnology provides a source of authoritative fundamentals, interdisciplinary knowledge and primary literature for researchers who want to fully understand how nano-technologies work. Covering all stages of analysis, from sample preparation to separation and detection, the book discusses the design and manufacturing technology of miniaturization and includes an entire section on safety risks, ethical, legal and social issues (ELSI), the economics of nanotechnologies, and a discussion on sustainability with respect to nano- and lab-on-chip technologies. This guide for students and researchers working on applications of nanotechnology in modern systems for analysis gives readers everything they need to know to bring their current practices up-to-date. Details the impacts of miniaturization and nanotechnology Includes coverage of the current challenges for scaling up nano-miniaturization design and manufacturing technology for analysis Provides the latest reference materials, including websites of interest and details on the latest research in every chapter


Miniaturization in Sample Preparation

Miniaturization in Sample Preparation
Author: Francisco Pena Pereira
Publisher: Walter de Gruyter GmbH & Co KG
Total Pages: 411
Release: 2014-01-01
Genre: Science
ISBN: 3110427265

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Miniaturization is a challenge thrown down to analytical chemistry. The replacement of conventional analytical systems by miniaturized alternatives during the last years is noticeable. Specifically, the miniaturization of traditional sample preparation techniques (e.g., solid-phase extraction or solvent extraction) led to the development of environmentally benign analytical methods. This book aims to provide an overview of the challenges and achievements inthe application of the miniaturized sample preparation methods in analytical laboratories. It includes both theoretical and practical aspects of miniaturized sample preparation approaches and hence should be of interest to researchers, students and teachers of analytical and bioanalytical chemistry, environmental sciences and environmental engineering.


Miniaturization and Mass Spectrometry

Miniaturization and Mass Spectrometry
Author: Séverine Le Gac
Publisher: Royal Society of Chemistry
Total Pages: 333
Release: 2009
Genre: Science
ISBN: 085404129X

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Focussing on mass spectrometry, this book illustrates how microfluidics and lab-on-a-chip devices satisfy the need for miniaturized, enhanced chemical analysis.


Handbook of Solid Phase Microextraction

Handbook of Solid Phase Microextraction
Author: Janusz Pawliszyn
Publisher: Elsevier
Total Pages: 497
Release: 2011-12-01
Genre: Science
ISBN: 0123914493

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The relatively new technique of solid phase microextraction (SPME) is an important tool to prepare samples both in the lab and on-site. SPME is a "green" technology because it eliminates organic solvents from analytical laboratory and can be used in environmental, food and fragrance, and forensic and drug analysis. This handbook offers a thorough background of the theory and practical implementation of SPME. SPME protocols are presented outlining each stage of the method and providing useful tips and potential pitfalls. In addition, devices and fiber coatings, automated SPME systems, SPME method development, and In Vivo applications are discussed. This handbook is essential for its discussion of the latest SPME developments as well as its in depth information on the history, theory, and practical application of the method. Practical application of Solid Phase Microextraction methods including detailed steps Provides history of extraction methods to better understand the process Suitable for all levels, from beginning student to experienced practitioner


Sample Preparation with Nanomaterials

Sample Preparation with Nanomaterials
Author: Chaudhery Mustansar Hussain
Publisher: John Wiley & Sons
Total Pages: 304
Release: 2021-04-06
Genre: Science
ISBN: 352768560X

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Discover this timely, comprehensive, and up-to-date exploration of crucial aspects of the use of nanomaterials in analytical chemistry Sample Preparation with Nanomaterials: Next Generation Techniques for Sample Preparation delivers insightful and complete overview of recent progress in the use of nanomaterials in sample preparation. The book begins with an overview of special features of nanomaterials and their applications in analytical sciences. Important types of nanomaterials, like carbon nanotubes and magnetic particles, are reviewed and biological sample preparation and lab-on-a-chip systems are presented. The distinguished author places special emphasis on approaches that tend to green and reduce the cost of sample treatment processes. He also discusses the legal, economical, and toxicity aspects of nanomaterial samples. This book includes extensive reference material, like a complete list of manufacturers, that makes it invaluable for professionals in analytical chemistry. Sample Preparation with Nanomaterials offers considerations of the economic aspects of nanomaterials, as well as the assessment of their toxicity and risk. Readers will also benefit from the inclusion of: A thorough introduction to nanomaterials in the analytical sciences and special properties of nanomaterials for sample preparation An exploration of the mechanism of adsorption and desorption on nanomaterials, including carbon nanomaterials used as adsorbents Discussions of membrane applications of nanomaterials, surface enhanced raman spectroscopy, and the use of nanomaterials for biological sample preparation A treatment of magnetic nanomaterials, lab-on-a-chip nanomaterials, and toxicity and risk assessment of nanomaterials Perfect for analytical chemists, materials scientists, and process engineers, Sample Preparation with Nanomaterials: Next Generation Techniques for Sample Preparation will also earn a place in the libraries of analytical laboratories, universities, and companies who conduct research into nanomaterials and seek a one-stop resource for sample preparation.


Sampling and Sample Preparation in Field and Laboratory

Sampling and Sample Preparation in Field and Laboratory
Author: Janusz Pawliszyn
Publisher: Elsevier
Total Pages: 1170
Release: 2002-09-09
Genre: Science
ISBN: 9780444505118

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This title is the first comprehensive book on sampling and modern sample preparation techniques and has several main objectives: to facilitate recognition of sample preparation as both an integral part of the analytical process; to present a fundamental basis and unified theoretical approach for the professional development of sample preparation; to emphasize new developments in sample preparation technology; and to highlight the future impact of sample preparation on new directions in analytical science, particularly automation, miniaturization and field implementation. Until recently, there has been relatively little scientific interest in sampling and sample preparation, however this situation is presently changing as sampling and sample preparation become integral parts of the analytical process with their own unique challenges and research opportunities. Sampling and Sample Preparation for Field and Laboratory is an essential resource for all analytical chemists, and in particular those involved in method development. Not only does it cover the fundamental aspects of extraction, it also covers applications in various matrices and includes sampling strategies and equipment and how these can be integrated into the analytical process for maximum efficiency.


Sample Preparation Techniques in Analytical Chemistry

Sample Preparation Techniques in Analytical Chemistry
Author: Somenath Mitra
Publisher: John Wiley & Sons
Total Pages: 480
Release: 2004-04-07
Genre: Science
ISBN: 0471457825

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The importance of accurate sample preparation techniques cannot be overstated--meticulous sample preparation is essential. Often overlooked, it is the midway point where the analytes from the sample matrix are transformed so they are suitable for analysis. Even the best analytical techniques cannot rectify problems generated by sloppy sample pretreatment. Devoted entirely to teaching and reinforcing these necessary pretreatment steps, Sample Preparation Techniques in Analytical Chemistry addresses diverse aspects of this important measurement step. These include: * State-of-the-art extraction techniques for organic and inorganic analytes * Sample preparation in biological measurements * Sample pretreatment in microscopy * Surface enhancement as a sample preparation tool in Raman and IR spectroscopy * Sample concentration and clean-up methods * Quality control steps Designed to serve as a text in an undergraduate or graduate level curriculum, Sample Preparation Techniques in Analytical Chemistry also provides an invaluable reference tool for analytical chemists in the chemical, biological, pharmaceutical, environmental, and materials sciences.


Analytical Sample Preparation With Nano- and Other High-Performance Materials

Analytical Sample Preparation With Nano- and Other High-Performance Materials
Author: Rafael Lucena
Publisher: Elsevier
Total Pages: 572
Release: 2021-10-22
Genre: Science
ISBN: 0128221399

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Analytical Sample Preparation With Nano- and Other High-Performance Materials covers advanced sample treatment techniques and the new materials that can be used to boost their performance. The evolution of sample treatment over the last two decades has resulted in the development of new techniques and application of new materials. This is a must-have resource for those studying advanced analytical techniques and the role of high-performance materials in analytical chemistry. The book explains the underlying principles needed to properly understand sample preparation, and also examines the latest materials - including nanomaterials - that result in greater sensitivity and specificity. The book begins with a section devoted to all the various sample preparation techniques and then continues with sections on high-performance sorbents and high-performance solvents. Combines basic, fundamental principles and advanced concepts and applications for a comprehensive treatment of sample preparation with new materials Defines nano- and other high-performance materials in this context, including carbon nanoparticles, inorganic nanoparticles, ionic liquids, supramolecular solvents, and more Includes discussion of all the latest advancements and new findings in both techniques and materials used for proper sample preparation


Micro- and Nanotechnology Enabled Applications for Portable Miniaturized Analytical Systems

Micro- and Nanotechnology Enabled Applications for Portable Miniaturized Analytical Systems
Author: Sabu Thomas
Publisher: Elsevier
Total Pages: 440
Release: 2021-10-12
Genre: Technology & Engineering
ISBN: 0128237287

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Micro- and Nanotechnology Enabled Applications for Portable Miniaturized Analytical Systems outlines the basic principles of miniaturized analytical devices, such as spectrometric, separation, imaging and electrochemical miniaturized instruments. Concepts such as smartphone-enabled miniaturized detection systems and micro/nanomachines are also reviewed. Subsequent chapters explore the emerging application of these mobile devices for miniaturized analysis in various fields, including medicine and biomedicine, environmental chemistry, food chemistry, and forensic chemistry. This is an important reference source for materials scientists and engineers wanting to understand how miniaturization techniques are being used to create a range of efficient, sustainable electronic and optical devices. Miniaturization describes the concept of manufacturing increasingly smaller mechanical, optical, and electronic products and devices. These smaller instruments can be used to produce micro- and nanoscale components required for analytical procedures. A variety of micro/nanoscale materials have been synthesized and used in analytical procedures, such as sensing materials, sorbents, adsorbents, catalysts, and reactors. The miniaturization of analytical instruments can be applied to the different steps of analytical procedures, such as sample preparation, analytical separation, and detection, reducing the total cost of manufacturing the instruments and the needed reagents and organic solvents. Outlines how miniaturization techniques can be used to create new optical and electronic micro- and nanodevices Explores major application areas, including biomedicine, environmental science and security Assesses the major challenges of using miniaturization techniques