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Hands on NMR

Hands on NMR
Author: William S. Price
Publisher:
Total Pages: 500
Release: 2021-05-17
Genre: Science
ISBN: 9781788010887

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Presenting important practical aspects of NMR spectroscopy, this book will be useful for explaining and facilitating the successful set up of a wide variety of NMR experiments. It will enlighten readers with the relevant information on the basic concepts in NMR, how it works, and how to trouble-shoot artefacts that may be encountered. A short introductory chapter on some basic theory and key concepts will precede chapters on more practical aspects e.g. instrumentation, sample preparation, experimentation and data processing. Several practical case experiments covering various fields and including details on the pitfalls, tips and recommendations are presented next. Lastly, detailed chapters on other important practical aspects such as artefacts, spectral prediction, databases and safety are included. Bringing books that present practical NMR up to date, this book fills a gap in the literature and provides a new comprehensive practical NMR book for teaching and research at all levels - graduates, postgraduates, industry and research.


NMR Spectroscopy in Food Analysis

NMR Spectroscopy in Food Analysis
Author: Apostolos Spyros
Publisher: Royal Society of Chemistry
Total Pages: 311
Release: 2015-10-20
Genre: Technology & Engineering
ISBN: 1782625666

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During the last two decades, the use of NMR spectroscopy for the characterization and analysis of food materials has flourished, and this trend continues to increase today. Currently, there exists no book that fulfils specifically the needs of food scientists that are interested in adding or expanding the use of NMR spectroscopy in their arsenal of food analysis techniques. Current books and monographs are rather addressed to experienced researchers in food analysis providing new information in the field. This book, written by acknowledged experts in the field, fills the gap by offering a day to day NMR guide for the food scientist, affording not only the basic theoretical aspects of NMR spectroscopy, but also practical information on sample preparation, experimental conditions and data analysis. Current developments in the field covered in this book are the availability of solid state NMR experiments such as CP/MAS and more importantly HR-MAS NMR for the analysis of semisolid foods, and the increasing use of chemometrics to analyze NMR data in food metabonomics. Moreover, this book contains an up to date discussion of MRI in food analysis including topics such as food processing and natural changes in food such as ripening. The book is a compact and complete source of information for food scientists who wish to apply methodologies based on NMR spectroscopy in food analysis. It contains information so far scattered in the primary literature, in NMR treatises and food analysis books, in a concise format that makes it appealing to food scientists who have no or minimal experience in magnetic resonance techniques. The inclusion of practical information about NMR instrumentation, experiment setup, acquisition and spectral analysis for the study of different food categories make this book a hands-on manual for food scientists wishing to implement novel NMR spectroscopy-based analytical techniques in their field.


Practical NMR Spectroscopy Laboratory Guide: Using Bruker Spectrometers

Practical NMR Spectroscopy Laboratory Guide: Using Bruker Spectrometers
Author: John S. Harwood
Publisher: Academic Press
Total Pages: 137
Release: 2015-10-28
Genre: Science
ISBN: 0128007192

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Practical NMR Spectroscopy Laboratory Guide is designed to provide non-expert NMR users, typically graduate students in chemistry, an introduction to various facets of practical solution-state NMR spectroscopy. Each chapter offers a series of hands-on exercises, introducing various NMR concepts and experiments and guiding the reader in running these experiments using an NMR spectrometer. The book is written for use with a Bruker NMR spectrometer running TopSpin software versions 1 or 2. This practical resource functions both as a text for instructors of a practical NMR course and also as a reference for spectrometer administrators or NMR facility directors when doing user training. This guide serves as serve as excellent, practical resource on its own or as a companion book to Timothy Claridge’s High-Resolution NMR Techniques in Organic Chemistry, 2nd Edition (Elsevier, 2009). Written by experts in solution-state NMR spectroscopy Provides step-by-step instructions for more than 50 activities using a Bruker NMR spectrometer Includes detailed appendices and sample questions for lab reports


NMR Spectroscopy of Polymers

NMR Spectroscopy of Polymers
Author: Tatsuki Kitayama
Publisher: Springer Science & Business Media
Total Pages: 231
Release: 2013-03-09
Genre: Technology & Engineering
ISBN: 3662089823

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Based on the authors ́ extensive experimental experience, NMR Spectroscopy of Polymers explains the practical use of NMR spectroscopy in polymer chemistry.


Essential Practical NMR for Organic Chemistry

Essential Practical NMR for Organic Chemistry
Author: S. A. Richards
Publisher: John Wiley & Sons
Total Pages: 293
Release: 2023-05-01
Genre: Science
ISBN: 1119844800

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A hands-on resource advocating an ordered approach to gathering and interpreting NMR data The second edition of Essential Practical NMR for Organic Chemistry delivers a pragmatic and accessible text demonstrating an ordered approach to gathering and interpreting NMR data. In this informal guide, you’ll learn to make sense of the high density of NMR information through the authors’ problem-solving strategies and interpretations. The book also discusses critical aspects of NMR theory, as well as data acquisition and processing strategy. It explains the use of NMR spectroscopy for dealing with problems of small organic molecule structural elucidation and includes a brand-new chapter on Nitrogen-15 NMR. Readers will also find: Strategies for preparing a sample, spectrum acquisition, processing, and interpreting your spectrum Fulsome discussions of Carbon-13 NMR spectroscopy Practical treatments of quantification, safety procedures, and relevant software An ideal handbook for anyone involved in using NMR to solve structural problems, this latest edition of Essential Practical NMR for Organic Chemistry will be particularly useful for chemists running and looking at their own NMR spectra, as well as those who work in small molecule NMR. It will also earn a place in the libraries of undergraduate and post-graduate organic chemistry students.


Basic 1H- and 13C-NMR Spectroscopy

Basic 1H- and 13C-NMR Spectroscopy
Author: Metin Balci
Publisher: Elsevier
Total Pages: 441
Release: 2005-01-19
Genre: Science
ISBN: 0080525539

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Nuclear Magnetic Resonance (NMR) spectroscopy is a powerful and theoretically complex analytical tool. Basic 1H- and 13C-NMR Spectroscopy provides an introduction to the principles and applications of NMR spectroscopy. Whilst looking at the problems students encounter when using NMR spectroscopy, the author avoids the complicated mathematics that are applied within the field. Providing a rational description of the NMR phenomenon, this book is easy to read and is suitable for the undergraduate and graduate student in chemistry. Describes the fundamental principles of the pulse NMR experiment and 2D NMR spectra Easy to read and written with the undergraduate and graduate chemistry student in mind Provides a rational description of NMR spectroscopy without complicated mathematics


Fundamentals of Protein NMR Spectroscopy

Fundamentals of Protein NMR Spectroscopy
Author: Gordon S. Rule
Publisher: Springer Science & Business Media
Total Pages: 543
Release: 2006-02-16
Genre: Science
ISBN: 1402035004

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NMR spectroscopy has proven to be a powerful technique to study the structure and dynamics of biological macromolecules. Fundamentals of Protein NMR Spectroscopy is a comprehensive textbook that guides the reader from a basic understanding of the phenomenological properties of magnetic resonance to the application and interpretation of modern multi-dimensional NMR experiments on 15N/13C-labeled proteins. Beginning with elementary quantum mechanics, a set of practical rules is presented and used to describe many commonly employed multi-dimensional, multi-nuclear NMR pulse sequences. A modular analysis of NMR pulse sequence building blocks also provides a basis for understanding and developing novel pulse programs. This text not only covers topics from chemical shift assignment to protein structure refinement, as well as the analysis of protein dynamics and chemical kinetics, but also provides a practical guide to many aspects of modern spectrometer hardware, sample preparation, experimental set-up, and data processing. End of chapter exercises are included to emphasize important concepts. Fundamentals of Protein NMR Spectroscopy not only offer students a systematic, in-depth, understanding of modern NMR spectroscopy and its application to biomolecular systems, but will also be a useful reference for the experienced investigator.


50 and More Essential NMR Experiments

50 and More Essential NMR Experiments
Author: Matthias Findeisen
Publisher: John Wiley & Sons
Total Pages: 322
Release: 2013-11-04
Genre: Science
ISBN: 3527334831

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This book is the perfect link for learning how to perform the experiments after only having studied theory. In eight chapters more than 50 essential NMR experiments are described in detail. Special focus is put on the organic set of NMR spectra (1H, 13C-APT, COSY, NOESY, HSQC and HMBC). Different chapters deal with advanced organic NMR, selective methods, heteronuclear NMR, relaxation and diffusion measurements, organic applications and maintenance. Every experiment has a section providing the reader with the purpose and scope of the specific experiment. Every experiment is concluded with the spectrum as it is obtained under the conditions described. Questions and comments enable the reader to check their understanding. The authors are very experienced and the whole book is in full color, which enhances the reading experience and makes the spectra and other figures easier to understand. This book is strongly recommended for all students and researchers who are involved in the structural elucidation of chemical compounds both in practical education and in pursuing research, in particular if they handle an NMR spectrometer.


NMR Spectroscopy Explained

NMR Spectroscopy Explained
Author: Neil E. Jacobsen
Publisher: John Wiley & Sons
Total Pages: 640
Release: 2007-09-10
Genre: Science
ISBN: 0470173343

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NMR Spectroscopy Explained : Simplified Theory, Applications and Examples for Organic Chemistry and Structural Biology provides a fresh, practical guide to NMR for both students and practitioners, in a clearly written and non-mathematical format. It gives the reader an intermediate level theoretical basis for understanding laboratory applications, developing concepts gradually within the context of examples and useful experiments. Introduces students to modern NMR as applied to analysis of organic compounds. Presents material in a clear, conversational style that is appealing to students. Contains comprehensive coverage of how NMR experiments actually work. Combines basic ideas with practical implementation of the spectrometer. Provides an intermediate level theoretical basis for understanding laboratory experiments. Develops concepts gradually within the context of examples and useful experiments. Introduces the product operator formalism after introducing the simpler (but limited) vector model.


Dynamic NMR Spectroscopy

Dynamic NMR Spectroscopy
Author:
Publisher: Springer Science & Business Media
Total Pages: 220
Release: 2012-12-06
Genre: Science
ISBN: 3642669611

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Since the first successful NMR experiments in 1946 it was well appreciated that dynamic processes play an important role in the NMR spectroscopy of bulk matter [1]. Early theories on the dependence of the relaxation parameters Tl and T2 on the motions of nuclear spins were successful in explaining the dipolar broadening of the NMR signal in solids and the motional narrowing in liquids [2]. With the discovery of chemical shifts and spin-spin couplings another type of dynamical process affect ing the NMR line shape became apparent, the chemical exchange. As a consequence, dynamical NMR studies split into two groups differing not only in the dynamical topics but also in the method of investigation: physical studies of the motion of spins in liquids and solids by measurement of the relaxation times of single resonances and, on the other hand, chemical studies based on band shape analysis of NMR spectra recorded under steady state conditions. The two fields of research lost some of their basic differences with the development of the Fourier transform NMR method [3], which allows the measurement of relaxation times of different resonances at the same time, i. e. the study of differential motional behavior of different parts of mole cules, thus providing a new tool in conformational analyses. For example, informa tion can be obtained by this method on the relative importance of overall motions and internal motions [4].