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Exploring Fast Neutron Computed Tomography for Non-destructive Evaluation of Additive Manufactured Parts

Exploring Fast Neutron Computed Tomography for Non-destructive Evaluation of Additive Manufactured Parts
Author: Ibrahim Oksuz
Publisher:
Total Pages: 0
Release: 2022
Genre: Neutrons
ISBN:

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Neutron imaging is one of the most powerful non-invasive investigation modalities that finds many applications in various fields such as nuclear industry, homeland security, battery research, and archeology. It provides information about the internal structures of an object as neutrons are absorbed and transmitted at different levels in the object in question. It is complementary to X-ray imaging due to the different interaction mechanisms of X-ray and neutrons with materials. Neutron imaging applications can employ neutrons with different energies. Fast (MeV) neutrons have some advantages such as causing less radioactive transmutation in samples and providing deeper penetration which allows for exploring thicker and denser samples. It also provides good contrast images of objects made of a mix of hydrogenous and metallic elements. With the advent of the CCD technology, new opportunities have become available to perform neutron radiography, which provides 2D images of objects, and tomography, which yields information about objects in 3D, more efficiently. Digital neutron radiography allows the collection and storage the information in a digital environment, which enables a better and quicker data analysis. However, performing neutron imaging requires a well-characterized neutron source and a proper neutron imager, especially if fast neutrons are utilized as their interaction cross sections with materials are relatively smaller. This work explores the advancement of the fast neutron radiograph and tomography. The work includes studies comprising characterizing neutron detectors for fast imaging application, characterizing a fast neutron beam facility, performing fast neutron tomography using various imaging phantoms, and investigating spatial resolution in a fast neutron imaging system. In one study, Polyvinyl Toluene (PVT) (C9H10) based plastic scintillators with different dimensions and flours were investigated in terms of their relative light outputs and spatial resolutions. Due to high hydrogen concentration, PVT scintillators would be a suitable candidate since fast neutrons deposit higher energy as they interact mainly via elastic scattering reactions. This study resulted that thicker scintillators yield higher light output due to a higher amount of scintillation materials whereas they performed worse in spatial resolution because of more neutrons and light scattering. Another study was related to characterizing the Ohio State University Research Reactor (OSURR)’ recently built fast neutron beam facility. Models of the beamline and beam stop were created, and Monte-Carlo simulations were performed to determine the neutron energy spectrum, neutron, and gamma-ray flux, and dose rate distributions. Various thermal neutron filters were investigated, and Cadmium ratios that they provide were experimentally determined. Gamma-ray content in the beam was obtained using Optically Stimulated Luminescence (OSL) dosimeters. Another study investigates fast neutron computed tomography (nCT) using custom-made multi-material complex objects. Total nCT data collection time was as low as 2 hours for some objects. Various materials were resolved in 3D reconstructed images of the objects. Low-Z materials comprising the objects were revealed while being shielded behind high-Z materials. The last study in this work is about the investigation of the possible effects on the system's spatial resolution in a fast neutron imaging system. Results showed that the thicker imaging objects deteriorate the spatial resolution due to the neutron scattering. Simulations provided that the neutron interaction kinematics in PVTs would also degrade the spatial resolution.


Neutron Imaging

Neutron Imaging
Author: Dinesh K. Aswal
Publisher: Springer Nature
Total Pages: 368
Release: 2022-04-12
Genre: Science
ISBN: 9811662738

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This book comprehensively presents the concepts of neutron physics and imaging including neutron properties, neutron matter interaction, neutron imaging, comparison with X-ray and physics and design of neutron sources. It discusses how neutron imaging has gained importance as a powerful non-destructive technique to understand the internal structures of materials/engineered components in wide range of industries by increasing their applicability and efficiency. The book also covers the topics of neutron optics and detectors, basic principles of neutron radiography and tomography, related standards, safety, metrology and regulations in neutron imaging. The book presents applications of neutron imaging in the areas of aerospace industry, nuclear power and manufacturing industry, materials science and engineering, geomechanics, national security, biological, and medical domain. Given its scope, the book will be highly beneficial for postgraduate students, researchers and industry professionals working in the area of engineering and physics, especially non-destructive testing and non-destructive evaluation through neutron imaging.


Practical Applications of Neutron Radiography and Gaging

Practical Applications of Neutron Radiography and Gaging
Author: Symposium on Practical Applications of Neutron Radiography and Gaging
Publisher: ASTM International
Total Pages: 336
Release: 1976
Genre: Technology & Engineering
ISBN: 9780803105355

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Neutron Radiography

Neutron Radiography
Author: Garbe,U.
Publisher: Materials Research Forum LLC
Total Pages: 316
Release: 2020-02-05
Genre: Technology & Engineering
ISBN: 1644900572

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Neutron radiography represents a powerful non-destructive testing technique that is still very much in development. The book reveals the amazing diversity of scientific and industrial applications of this technique, the advancements of the state-of-art neutron facilities, the latest method developments, and the expected future of neutron imaging.


Neutron Radiography

Neutron Radiography
Author: Harold Berger
Publisher:
Total Pages: 102
Release: 1998
Genre: Neutron radiography
ISBN:

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Simulated Neutron Tomography for Nondestructive Assays

Simulated Neutron Tomography for Nondestructive Assays
Author:
Publisher:
Total Pages:
Release: 1979
Genre:
ISBN:

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The results of an on-going research project to assess the use of resonance-neutron computed-tomography for the assay of fissile materials will be discussed. A simulation study has indicated the potential value of this technique for the nondestructive inspection of a standard to be fabricated by the National Bureau of Standards.


Development of a Neutron Radiography and Computed Tomography System at a University Research Reactor

Development of a Neutron Radiography and Computed Tomography System at a University Research Reactor
Author: Derek Anderson Haas
Publisher:
Total Pages: 130
Release: 2006
Genre: Neutron radiography
ISBN:

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Neutron radiography is a non-destructive analysis tool that complements X-ray transmission radiography. The use of neutrons provides the ability to image the interior of an object that has a metal core of steel or lead that would shield the interior from X-ray inspection. Neutron tomography is the use of a set of images of a single sample taken at various angles to produce a three dimensional rendition of the sample that greatly increases the effectiveness of neutron radiography as a non-destructive testing tool. A neutron radiography and tomography system has been built at the 1.1 MW TRIGA Mark II nuclear research reactor at The University of Texas at Austin in the Nuclear Engineering Teaching Lab. The Texas Neutron Imaging Facility is located on beam port five of the reactor and is housed in a shielding cave made of concrete to minimize radiation dose to users. The system itself integrates a sample positioning system and neutron sensitive camera through the use of a control code written in National Instruments Labview software. The code was written to increase the efficiency of the imaging process and to provide flexibility in the system. Precise sample positioning and timing of image acquisition provided by the code allows for the collection of data that can be used in computed tomography. The system has produced results in the form of radiographs and 3-D reconstructions of sample objects.


Three New Nondestructive Evaluation Tools Based on High Flux Neutron Sources

Three New Nondestructive Evaluation Tools Based on High Flux Neutron Sources
Author:
Publisher:
Total Pages: 8
Release: 1997
Genre:
ISBN:

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Nondestructive evaluation methods and systems based on specific attributes of neutron interactions with materials are being developed. The special attributes of neutrons are low attenuation in most engineering materials, strong interaction with low Z elements, and epithermal neutron absorption resonances. The three methods under development at ORNL include neutron based tomography and radiography; through thickness, nondestructive texture mapping; and internal, noninvasive temperature measurement. All three techniques require high flux sources such as the High Flux Isotope Reactor, a steady state source, or the Oak Ridge Electron Linear Accelerator, a pulsed neutron source. Neutrons are quite penetrating in most engineering materials and thus can be useful to detect internal flaws and features. Hydrogen atoms, such as in a hydrocarbon fuel, lubricant, or a metal hydride, are relatively opaque to neutron transmission and thus neutron based tomography/radiography is ideal to image their presence. Texture, the nonrandom orientation of crystalline grains within materials, can be mapped nondestructively using neutron diffraction methods. Epithermal neutron resonance absorption is being studied as a noncontacting temperature sensor. This paper highlights the underlying physics of the methods, progress in development, and the potential benefits for science and industry of the three facilities.


Characterization of a Neutron Imaging Platform Utilizing a Compact Electronic Neutron Generator for Evaluation of Analog and Digital Neutron Imaging Methods and Techniques

Characterization of a Neutron Imaging Platform Utilizing a Compact Electronic Neutron Generator for Evaluation of Analog and Digital Neutron Imaging Methods and Techniques
Author: Michael James Taylor
Publisher:
Total Pages: 0
Release: 2019
Genre:
ISBN:

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Unlike X-Rays that interact strongly with the electron cloud surrounding atoms, neutrons interact very weakly with these electrons, but quite strongly with the nucleus of the atom. X-Rays follow a nearly linear trend of decreasing transmission as the atomic number of the element increases. Neutrons follow no such behavior and certain isotopes of elements such as lithium, boron, cadmium, and gadolinium interact very strongly with neutrons, unlike dense elements such as lead or tungsten. This gives neutrons a unique probing capability where X-Rays do not suffice. Neutron imaging is widely used in the commercial sector for munitions and critical aerospace component inspection as well as in the research realm for biological forensics, cultural heritage providence studies, and capturing repetitive processes such as cyclical fluid motion in rotating motors. Current neutron sources are typically nuclear reactors and spallation sources that provide incredibly high neutron yields and flux for the images, leading to reduced image times and/or high spatial resolution as well as new imaging techniques such as computed tomography, polarized neutron imaging, and phase contrast imaging. However, such sources are very expensive, require thorough regulatory oversight, and pose biological hazards from spent nuclear materials. Smaller sources such as sealed tube deuterium-deuterium or deuterium-tritium sources can allow for in-field inspection at a fraction of the cost of a reactor, but don't necessarily provide fast image acquisitions or adequate image quality. This thesis explores a system that is intended to fill the space between weak portable devices and strong, costly, immobile ones. An accelerator-based neutron generator has been designed and manufactured by Phoenix LLC in Madison, WI. This system operates on the principle of deuterium-deuterium fusion, which releases a free 2.45MeV (nominal) neutron in the fusion process. The system can be installed and commissioned in different locations throughout its lifetime and provides for in-field or commercial inspection of components. It has a neutron yield several orders of magnitude higher than sealed-tube neutron sources. The goal herein was to: enhance the performance of the neutron generator through careful beamline design from the source to the target to obtain the maximum neutron yield, optimize the geometry of the neutron moderator and collimator to maximize the imaging metrics of a thermalized and collimated neutron beam free of background gamma and fast neutron radiation contamination, and find efficient neutron detector solutions that can capture high-quality neutron images. Monte Carlo simulations were extensively employed for these optimization efforts. The system has been shown to produce high quality neutron radiographs in terms of contrast, noise, and resolution, using many different techniques for imaging. Many materials were explored for moderation and shielding, and many neutron detectors were researched and experimented with to demonstrate advantages and disadvantages for their use on the Phoenix neutron imaging system. Sample images will be shown and discussed including conventional radiography using medical, industrial, and photographic film, 2-dimension digital imaging using pixelated cameras such as Charge Coupled Devices (CCD), Complementary Metal Oxide Semiconductors (CMOS), amorphous Silicon (aSi), and Computed Radiography (CR). Neutron Computed Tomography (nCT) is demonstrated as a 3-dimensional imaging technique as well. Case studies will be discussed and options for further optimization for collimator, moderator, and detector designs will be outlined. Recommendations for future research will be discussed in the final chapter.