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Basic Multidimensional Gas Chromatography

Basic Multidimensional Gas Chromatography
Author:
Publisher: Academic Press
Total Pages: 332
Release: 2020-03-20
Genre: Science
ISBN: 0128137460

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Basic Multidimensional Gas Chromatography is aimed at the next generation of multidimensional gas chromatography users who will require basic training in the fundamentals of both GC and GCxGC. This book fills the current need for an inexpensive, straightforward guidebook to get new users started. It will help new users determine when to add or purchase a multidimensional system and teach them to optimize and maximize the capability of each system. Readers will also learn to select specific modes for each portion of a multidimensional analysis. This ideal resource is a concise, hard-hitting text that provides the facts needed to get users up and running. Provides a comprehensive and fundamental introduction to multidimensional gas chromatography Assists readers in determining when to add or purchase a multidimensional system Explains how a given system can be used to its maximum capacity and how users should choose specific modes for different portions of multidimensional analysis


Fire Debris Analysis

Fire Debris Analysis
Author: Eric Stauffer
Publisher: Academic Press
Total Pages: 683
Release: 2007-12-10
Genre: Law
ISBN: 0080556264

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The study of fire debris analysis is vital to the function of all fire investigations, and, as such, Fire Debris Analysis is an essential resource for fire investigators. The present methods of analysis include the use of gas chromatography and gas chromatography-mass spectrometry, techniques which are well established and used by crime laboratories throughout the world. However, despite their universality, this is the first comprehensive resource that addresses their application to fire debris analysis. Fire Debris Analysis covers topics such as the physics and chemistry of fire and liquid fuels, the interpretation of data obtained from fire debris, and the future of the subject. Its cutting-edge material and experienced author team distinguishes this book as a quality reference that should be on the shelves of all crime laboratories. Serves as a comprehensive guide to the science of fire debris analysis Presents both basic and advanced concepts in an easily readable, logical sequence Includes a full-color insert with figures that illustrate key concepts discussed in the text


Comprehensive Two Dimensional Gas Chromatography

Comprehensive Two Dimensional Gas Chromatography
Author: Lourdes Ramos
Publisher: Elsevier
Total Pages: 328
Release: 2009-07-22
Genre: Science
ISBN: 9780080932699

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The book reviews the basic concepts and highlights the most relevant advances and developments that have taken place in the field of comprehensive two dimensional gas chromatography (GC x GC) since its introduction in 1991. The several instrumental and technical approaches assayed and developed during these seventeen years and that have contributed to the development of this powerful separation technique and to its increasing application in many areas is explained and comprehensively illustrated through a number of chapters devoted these specific topics. More specialized aspects of the technique, including theoretical aspects, modelization of the chromatographic process, software developments, and alternative couplings is also covered. Finally, special attention is paid to data treatment, for both qualitative and quantitative analysis. This book will be a practical resource that will explain from basic to specialized concepts of GC x GC and will show the current state-of-the-art and discuss future trends of this technique. Outlines basic concepts and principles of GCxGC technique for non-specialists to apply the technique to their research Provides detailed descriptions of recent technical advances and serves as an instructional guide in latest applications in GCxGC Sets the scene for possible future development and alternative new applications of technique


Oil in the Sea III

Oil in the Sea III
Author: National Research Council
Publisher: National Academies Press
Total Pages: 278
Release: 2003-03-14
Genre: Science
ISBN: 0309084385

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Since the early 1970s, experts have recognized that petroleum pollutants were being discharged in marine waters worldwide, from oil spills, vessel operations, and land-based sources. Public attention to oil spills has forced improvements. Still, a considerable amount of oil is discharged yearly into sensitive coastal environments. Oil in the Sea provides the best available estimate of oil pollutant discharge into marine waters, including an evaluation of the methods for assessing petroleum load and a discussion about the concerns these loads represent. Featuring close-up looks at the Exxon Valdez spill and other notable events, the book identifies important research questions and makes recommendations for better analysis ofâ€"and more effective measures againstâ€"pollutant discharge. The book discusses: Inputâ€"where the discharges come from, including the role of two-stroke engines used on recreational craft. Behavior or fateâ€"how oil is affected by processes such as evaporation as it moves through the marine environment. Effectsâ€"what we know about the effects of petroleum hydrocarbons on marine organisms and ecosystems. Providing a needed update on a problem of international importance, this book will be of interest to energy policy makers, industry officials and managers, engineers and researchers, and advocates for the marine environment.


Practical Gas Chromatography

Practical Gas Chromatography
Author: Katja Dettmer-Wilde
Publisher: Springer
Total Pages: 904
Release: 2014-11-05
Genre: Science
ISBN: 3642546404

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Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered.


Characterization of Odorant Patterns by Comprehensive Two-Dimensional Gas Chromatography

Characterization of Odorant Patterns by Comprehensive Two-Dimensional Gas Chromatography
Author: Chiara Emilia Irma Cordero
Publisher: Elsevier
Total Pages: 442
Release: 2022-02-18
Genre: Science
ISBN: 0323988814

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The volume has as primary focus multidimensional gas chromatography (heart-cutting systems, comprehensive 2D-GC systems and hybrid solutions) and its characteristic features for in depth investigation of complex fractions of odor-active volatiles. Contributions, from outstanding researchers in the field from Academia and industry, cover fundamentals aspects on the physiology of olfaction, the strategies to identify key-odorants from the bulk of detectable volatiles (sensomics), the principles of operation of multidimensional analytical platforms (i.e., comprehensive two-dimensional gas chromatography - GC×GC; heart-cut 2D-GC, hybrid systems), and the fundamental role of mass spectrometry in providing reliable and informative data. Insights on new systems design and configurations are also provided, including sample preparation and data processing strategies, as important steps of the whole analytical process. Real-world examples cover food volatiles, complex aroma mixtures, odors emitted from industrial plants, volatiles of interest in forensic and medical applications. Providing insights on fundamental aspects and advances in analytical platforms design and work-flows implementation for volatiles and odorants patterns detection in key-application areas Up-dates on the most modern and advanced solutions to isolate, detect and characterize complex odorant patterns by multidimensional analytical techniques Critical overview on main application areas where odors have a key-information role: food aroma and flavor industry, industrial environments, forensic and clinical applications


Multidimensional Chromatography

Multidimensional Chromatography
Author: Luigi Mondello
Publisher: John Wiley & Sons
Total Pages: 464
Release: 2002-02-15
Genre: Science
ISBN: 9780471988694

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Mehrdimensionale Chromatographie im analytischen Labor: Dieses Buch bespricht erstmals alle gängigen Verfahren sowie Anwendungen auf verschiedensten Gebieten, von der Pharmazie, Biologie und Chemie bis hin zur Umwelttechnik und erdölverarbeitender Industrie. Die Autoren sind selbst aktiv in der einschlägigen Forschung tätig.


Characterization of Odorant Patterns by Comprehensive Two-Dimensional Gas Chromatography

Characterization of Odorant Patterns by Comprehensive Two-Dimensional Gas Chromatography
Author:
Publisher: Elsevier
Total Pages: 444
Release: 2022-02-16
Genre: Science
ISBN: 0323988822

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The volume has as primary focus multidimensional gas chromatography (heart-cutting systems, comprehensive 2D-GC systems and hybrid solutions) and its characteristic features for in depth investigation of complex fractions of odor-active volatiles. Contributions, from outstanding researchers in the field from Academia and industry, cover fundamentals aspects on the physiology of olfaction, the strategies to identify key-odorants from the bulk of detectable volatiles (sensomics), the principles of operation of multidimensional analytical platforms (i.e., comprehensive two-dimensional gas chromatography – GC×GC; heart-cut 2D-GC, hybrid systems), and the fundamental role of mass spectrometry in providing reliable and informative data. Insights on new systems design and configurations are also provided, including sample preparation and data processing strategies, as important steps of the whole analytical process. Real-world examples cover food volatiles, complex aroma mixtures, odors emitted from industrial plants, volatiles of interest in forensic and medical applications. Providing insights on fundamental aspects and advances in analytical platforms design and work-flows implementation for volatiles and odorants patterns detection in key-application areas Up-dates on the most modern and advanced solutions to isolate, detect and characterize complex odorant patterns by multidimensional analytical techniques Critical overview on main application areas where odors have a key-information role: food aroma and flavor industry, industrial environments, forensic and clinical applications


Principles and Practice of Analytical Techniques in Geosciences

Principles and Practice of Analytical Techniques in Geosciences
Author: Kliti Grice
Publisher:
Total Pages: 393
Release: 2015
Genre: Science
ISBN: 9781782625025

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The pace of revolution in analytical chemistry in the field of Geosciences has been dramatic over the recent decades and includes fundamental developments that have become common place in many related and unrelated disciplines. The analytical tools (nano to macro-scale from stable to radioactive isotopes to synchrotron imaging) used have been applied to wide-ranging applications from inorganic to organic geochemistry, biodiversity and chronological tools, to build an understanding of how the Earth system evolved to its present state. This book will provide an essential guide to exploring the earth's natural resources and changing climate by detection science. Individual chapters bring together expertise from across the globe to present a comprehensive outlook on the analytical technologies available to the geoscientist today. Experienced researchers will appreciate the broad treatment of the subject as a valuable reference, while students and those new to the field will quickly gain an appreciation of both the techniques at hand, and the importance of constructing, and analysing, the complex data sets they can generate.


Gas Chromatography-Mass Spectrometry with Cold EI: Leading the Way to the Future of GC-MS

Gas Chromatography-Mass Spectrometry with Cold EI: Leading the Way to the Future of GC-MS
Author: Aviv Amirav
Publisher: Scientific Research Publishing, Inc. USA
Total Pages: 265
Release: 2021-08-30
Genre: Science
ISBN: 1649971427

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Gas chromatography-mass spectrometry (GC-MS) with supersonic molecular beams (SMB) (also named GC-MS with Cold EI) is based on GC and MS interface with a SMB and on the electron ionization (EI) of vibrationally cold analytes in the SMB (hence the name Cold EI) in a contact-free fly-through ion source. Cold EI improves all the central GC-MS performance aspects and brings a broad range of important benefits thereby leading the way to the future of GC-MS. Cold EI provides enhanced molecular ions combined with effective library-basedsample identification. Sample identification is further improved by the use of powerful TAMI software that is based on isotope abundance analysis and improved quadrupole mass accuracy for the provision of the sample elemental formula from its molecular ion group of isotopologues.