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| Author | : Sara L. Kegler |
| Publisher | : |
| Total Pages | : 160 |
| Release | : 2002 |
| Genre | : Chemistry, Forensic |
| ISBN | : |
| Author | : Michael J. Telepchak |
| Publisher | : Springer Science & Business Media |
| Total Pages | : 398 |
| Release | : 2004-04-28 |
| Genre | : Medical |
| ISBN | : 1592592929 |
This complete laboratory reference manual explains the principles behind solid phase extraction (SPE) and provides readily reproducible protocols for solving extraction problems in forensic and clinical chemistry. Numerous actual chromatograms, based on original research and diverse applications, demonstrate the technique and the results that can be achieved. Extensive appendices allow fast access to frequently needed information on reagents, the preparation of solutions and buffers, milliequivalent and millimode calculations, buffers and pKa for SPE, and a complete RapidTrace® technical manual. Each proven protocol is described in step-by-step detail and contains an introduction outlining the principle behind the technique, lists of equipment and reagents, and tips on troubleshooting and on avoiding known pitfalls.
| Author | : Janusz Pawliszyn |
| Publisher | : Royal Society of Chemistry |
| Total Pages | : 680 |
| Release | : 1999 |
| Genre | : Science |
| ISBN | : 9780854045259 |
Solid Phase Microextraction (SPME) has been introduced as a modern alternative to current sample preparation technology, and has a wide range of applications. Focusing on quantitative aspects of analysis, Applications of Solid Phase Microextraction aims to describe these applications. In industry, practical uses of SPME can be found in environmental, food, pharmaceutical, clinical and forensic applications, all of which are described in this book. Important scientific applications such as reaction monitoring, characterization of coatings and distributions of analytes in natural multiphase systems are also discussed. Throughout there are descriptions of new technologies, including new coatings and interfaces for analytical instrumentation (SPME/LC and SPME/CE), automation and calibration processes. Written by internationally recognised experts, edited by the scientist involved in the research since its infancy, and encompassing a wide range of applications, this book will be ideal for anyone wishing to explore the feasibility of using SPME technology.
| Author | : Janusz Pawliszyn |
| Publisher | : Elsevier |
| Total Pages | : 497 |
| Release | : 2011-12-01 |
| Genre | : Science |
| ISBN | : 0123914493 |
The relatively new technique of solid phase microextraction (SPME) is an important tool to prepare samples both in the lab and on-site. SPME is a "green" technology because it eliminates organic solvents from analytical laboratory and can be used in environmental, food and fragrance, and forensic and drug analysis. This handbook offers a thorough background of the theory and practical implementation of SPME. SPME protocols are presented outlining each stage of the method and providing useful tips and potential pitfalls. In addition, devices and fiber coatings, automated SPME systems, SPME method development, and In Vivo applications are discussed. This handbook is essential for its discussion of the latest SPME developments as well as its in depth information on the history, theory, and practical application of the method. Practical application of Solid Phase Microextraction methods including detailed steps Provides history of extraction methods to better understand the process Suitable for all levels, from beginning student to experienced practitioner
| Author | : Janusz Pawliszyn |
| Publisher | : Royal Society of Chemistry |
| Total Pages | : 663 |
| Release | : 2023-03-24 |
| Genre | : Science |
| ISBN | : 1839166800 |
Solid Phase Microextraction (SPME) is a flexible and convenient sampling and sample preparation technique that extracts different kinds of analytes, including both volatile and non-volatile, without the use of a solvent. The technique facilitates fast, simple and automated determination of target analytes in a range of matrices. As it offers a green methodology, it is growing in popularity as an alternative tool in analytical chemistry to traditional methods. This book follows on in spirit from the editors' previous title, Applications of Solid Phase Microextraction and will introduce the reader to breakthrough methodologies and cutting edge applications. Although it assumes a good degree of SPME knowledge, an overview of the fundamentals is given before taking the reader through an update of the field. The reader will learn the basic principles and advantages of different SPME formats including the stir bar extraction techniques, thin film SPME, Bio-SPME, and new trends in different coatings. Applications in complex media, including food analysis, drug residues and bioanalysis are covered. Bringing together leading sample preparation academics from around the world, the editor has put together an informative new book, suitable for analytical chemists and practitioners utilising SPME tools in their research.
| Author | : Janusz Pawliszyn |
| Publisher | : John Wiley & Sons |
| Total Pages | : 266 |
| Release | : 1997-04-21 |
| Genre | : Science |
| ISBN | : 9780471190349 |
Gesetzliche Auflagen und ökonomische Erwägungen steigern den Bedarf an Propenpräparations- und -extraktionstechniken, die ohne toxische organische Lösungsmittel auskommen. Die hier erstmals in Buchform veröffentlichte Festphasen-Mikroextraktion (SPME) ist ein neuartiges Verfahren, das diesen Anforderungen entspricht und gegenwärtig apparativ umgesetzt wird. Der Erfinder selbst, ein international anerkannter Pionier auf dem Gebiet der lösungsmittelfreien Extraktion, erklärt theoretische Hintergründe und praktische Anwendungsmöglichkeiten. SPME ist einfach, kostengünstig, automatisierbar, zeit- und analytsparend. Interessant für Analytiker in Industrie und Forschung, für Spurenanalytik, Umwelt- und pharmazeutische Chemie.
| Author | : Sue Ann Wercinski |
| Publisher | : CRC Press |
| Total Pages | : 274 |
| Release | : 1999-07-09 |
| Genre | : Science |
| ISBN | : 9781439832387 |
An explanation of proven methods of chemical analysis, focusing on the myriad applications of solid phase microextraction (SPME) to laboratories performing high-sample throughput, quick sample turnaround time, low detection levels, and dirty sample matrices. It supplies commentary on developments in SPME technology from its inventor, Janusz Pawliszyn.
| Author | : Ben Benson |
| Publisher | : Nova Science Publishers |
| Total Pages | : 0 |
| Release | : 2018 |
| Genre | : Extraction (Chemistry) |
| ISBN | : 9781536145823 |
Conventional sample preparation techniques like solid phase extraction and liquid-liquid extraction prove to be tedious, time-consuming and oftentimes cumbersome. As a result, new sample techniques have been developed based on the two methods to optimize solvent consumption, miniaturize extraction and decrease environmental impact. In Solid-Phase Extraction: Procedure, Applications and Effects, the authors explore the recent developments and applications of solid phase microextraction techniques used in the preconcentration of personal care products.Following this, this collection addresses the use of chemical compounds for agriculture purposes which can cause the contamination of the environment. These contaminants can remain in the plant and soil or migrate from soil to water. As such, the authors suggest that the detection and quantification of pesticide residues in waters is of great concern.Membrane disk solid-phase extraction have been used to pretreat large-volume water samples because their large cross-section areas allow relatively high flow rates. Solid-phase extraction disks maintain their shape from the pretreatment process to the assaying step, making them useful for wet analyses as well as direct analyses.The closing chapter examines the development of the used solid-phase extraction sorbents since the introduction of the technique until today. Sample preparation always plays a key role in the chemical analysis of a variety of matrices and is the most time-consuming and complicated step of the entire analytical procedure.
| Author | : Gangfeng Ouyang |
| Publisher | : Springer |
| Total Pages | : 313 |
| Release | : 2016-11-24 |
| Genre | : Science |
| ISBN | : 366253598X |
This book offers comprehensive information on the developments and applications of the solid phase microextraction (SPME) technique. The first part of the book briefly introduces readers to the fundamentals of SPME, while subsequent sections describe the applications of SPME technique in detail, including environmental analysis (air, water, soil/sediments), food analysis (volatile/nonvolatile compounds), and bioanalysis (plants, animal tissues, body fluids). The advantages and future challenges of the SPME technique are also discussed. Including recent research advances and further developments of SPME, the book offers a practical reference guide and a valuable resource for researchers and users of SPME techniques. The target audience includes analytical chemists, environmental scientists, biological scientists, material scientists, and analysts, as well as students at universities/institutes in related fields. Dr. Gangfeng Ouyang is a Professor at the School of Chemistry and Chemical Engineering, Sun Yat-sen University, China. Dr. Ruifen Jiang is an Associate Professor at the School of Environment, Jinan University, China.
| Author | : Nigel J.K. Simpson |
| Publisher | : CRC Press |
| Total Pages | : 532 |
| Release | : 2000-03-15 |
| Genre | : Science |
| ISBN | : 9781420056242 |
Demonstrating the relationship of the basic theory of solid-phase extraction (SPE) to chromatography, this comprehensive reference illustrates how SPE techniques significantly contribute to the preparation of samples for a wide variety of analytical techniques. It provides step-by-step details on the applications of SPE to environmental matrices, broad-spectrum drug screening, veterinary drug abuse, pharmaceutical drug development, biological samples, and high-throughput screening. Written by world-renowned experts in the field, the book contains helpful reference charts, tables of solvent properties, selectivities, molecular acid/base properties, and more.
