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Acquisition of a Combined Scanning Near-Field Optical and Atomic Force Microscope

Acquisition of a Combined Scanning Near-Field Optical and Atomic Force Microscope
Author:
Publisher:
Total Pages: 0
Release: 2005
Genre:
ISBN:

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This project supported a new universal scanning microscope system combining near-field scanning optical microscopy (NSOM), conventional atomic force (AFM) microscopy, and confocal optical microscopy. To build a universal system capable of high-resolution topographical imaging concurrently with spectroscopic abilities, the authors have acquired several independent units and combined them into a custom-designed NSOM/AFM/Raman instrument. They have acquired an atomic force microscope (Multimode, Digital Instruments), a near-field scanning microscope (Aurora III, Digital Instruments, partially supported by NASA), and a SpectraPro Raman spectrograph from Roper. In addition to these major instruments, they acquired a number of supporting parts/instruments toward their goal of completion of the system and sample preparation, selection, and characterization for Raman studies (e.g., CCD camera, avalanche detectors, two lasers, optical parts, air table, fluorescence microscope, mini x-ray unit, etc). A post-doctoral Research Associate was in charge of putting all these parts together. The authors did not go with a single unit from WiTec because actual demonstrations did not show expected sensitivity. This report presents a description of the instrument and preliminary results obtained with it. The instrument was used to collect Raman spectra from patterned arrays of bent single wall carbon nanotubes and bundles (3 nm in diameter) and from freely suspended nanomembranes with encapsulated gold nanoparticles.


Atomic Force Microscopy, Scanning Nearfield Optical Microscopy and Nanoscratching

Atomic Force Microscopy, Scanning Nearfield Optical Microscopy and Nanoscratching
Author: Gerd Kaupp
Publisher: Springer Science & Business Media
Total Pages: 302
Release: 2006-10-24
Genre: Technology & Engineering
ISBN: 3540284729

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Making a clear distinction is made between nano- and micro-mechanical testing for physical reasons, this monograph describes the basics and applications of the supermicroscopies AFM and SNOM, and of the nanomechanical testing on rough and technical natural surfaces in the submicron range down to a lateral resolution of a few nm. New or improved instrumentation, new physical laws and unforeseen new applications in all branches of natural sciences (around physics, chemistry, mineralogy, materials science, biology and medicine) and nanotechnology are covered as well as the sources for pitfalls and errors. It outlines the handling of natural and technical samples in relation to those of flat standard samples and emphasizes new special features. Pitfalls and sources of errors are clearly demonstrated as well as their efficient remedy when going from molecularly flat to rough surfaces. The academic or industrial scientist learns how to apply the principles for tackling their scientific or manufacturing tasks that include roughness far away from standard samples.


Atomic Force Microscopy

Atomic Force Microscopy
Author: Armand Vance
Publisher:
Total Pages: 0
Release: 2016-04
Genre: Atomic force microscopy
ISBN: 9781681172125

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The atomic force microscope (AFM) is one kind of scanning probe microscopes (SPM). SPMs are designed to measure local properties, such as height, friction, magnetism, with a probe. To acquire an image, the SPM raster-scans the probe over a small area of the sample, measuring the local property simultaneously. The information is gathered by "feeling" or "touching" the surface with a mechanical probe. Piezoelectric elements that facilitate tiny but accurate and precise movements on (electronic) command enable very precise scanning. Compared to competitive technologies such as optical microscopy and electron microscopy, the major difference between these and the atomic-force microscope is that the latter does not use lenses or beam irradiation. Therefore, it does not suffer from a limitation of space resolution due to diffraction limit and aberration, and it is not necessary to prepare a space for guiding the beam (by creating a vacuum) or to stain the sample. Piezo-ceramics position the tip with high resolution. Piezoelectric ceramics are a class of materials that expand or contract when in the presence of a voltage gradient. Piezo-ceramics make it possible to create three-dimensional positioning devices of arbitrarily high precision. In contact mode, AFMs use feedback to regulate the force on the sample. The AFM not only measures the force on the sample but also regulates it, allowing acquisition of images at very low forces. The feedback loop consists of the tube scanner that controls the height of the tip; the cantilever and optical lever, which measures the local height of the sample; and a feedback circuit that attempts to keep the cantilever deflection constant by adjusting the voltage applied to the scanner. The atomic force microscope is a powerful tool that is invaluable if to measure incredibly small samples with a great degree of accuracy. Unlike rival technologies it does not require either a vacuum or the sample to undergo treatment that might damage it. At the limits of operation however, researchers have demonstrated atomic resolution in high vacuum and even liquid environments. The book entitled Atomic Force Microscopy covers the applications and theories of atomic force microscope.


Atomic Force Microscopy

Atomic Force Microscopy
Author: Victor Bellitto
Publisher: BoD – Books on Demand
Total Pages: 272
Release: 2012-03-23
Genre: Science
ISBN: 9535104144

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With the advent of the atomic force microscope (AFM) came an extremely valuable analytical resource and technique useful for the qualitative and quantitative surface analysis with sub-nanometer resolution. In addition, samples studied with an AFM do not require any special pretreatments that may alter or damage the sample and permits a three dimensional investigation of the surface. This book presents a collection of current research from scientists throughout the world that employ atomic force microscopy in their investigations. The technique has become widely accepted and used in obtaining valuable data in a wide variety of fields. It is impressive to see how, in a short time period since its development in 1986, it has proliferated and found many uses throughout manufacturing, research and development.


Scanning Tunneling Microscope and Atomic Force Microscopy

Scanning Tunneling Microscope and Atomic Force Microscopy
Author: Suchit Sharma
Publisher: GRIN Verlag
Total Pages: 21
Release: 2017-12-05
Genre: Technology & Engineering
ISBN: 3668588252

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Literature Review from the year 2015 in the subject Engineering - General, Indian Institute of Technology, Delhi, course: Mineral Engineering, language: English, abstract: Atomic-scale resolution is needed to study the arrangement of atoms in materials and advancing their understanding. Since the seventeenth-century optical microscopes using visible light as illumination source have led our quest to observe microscopic species but the resolution attainable reached physical limits due to the much longer wavelength of visible light. After the discovery of wave nature associated with particle bodies, a new channel of thought opened considering much shorter wavelength of particles and their special properties when interacting with the sample under observation. These particles i.e. electrons, neutrons and ions were developed in different techniques and were used as illumination sources. Herein, the development of scanning tunneling microscopy which used electrons to uncover irregularities in the arrangement of atoms in thin materials via the quantum mechanical phenomenon of electron tunneling became a sensational invention. Atomic Force Microscopy (AFM) is a development over STM which relied on measuring the forces of contact between the sample and a scanning probe which overcame the earlier technique only allowing conductors or pretreated surfaces for conducting to be observed. Since measuring contact forces between materials is a more fundamental approach that is equally but more sensitive than measuring tunneling current flowing between them, atomic force microscopy has been able to image insulators as well as semiconductors and conductors with atomic resolution by substituting tunneling current with an atomic contact force sensing arrangement, a delicate cantilever, which can image conductors and insulators alike via mechanical "touch" while running over surface atoms of the sample. AFM has seen a massive proliferation in hobbyist’s lab in form of ambient-condition scanning environment as opposed to an ultra-high vacuum of sophisticated labs and self-assembled instrumentations. The success of ATM as a cost-effective imaging tool with dramatically increased ease of conceptual understanding and use particularly with the assistance of significant computing power in the form of personal computers which offsets the computational difficulty of resolving experimental information which makes up for physical simplicity of instrument design has seen its proliferation to numerous labs in universities and technology companies worldwide.


Near-field Optics

Near-field Optics
Author: Society of Photo-optical Instrumentation Engineers
Publisher:
Total Pages: 178
Release: 1995
Genre: Science
ISBN:

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