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A Practical Guide to Total Reflection X-ray Fluorescence

A Practical Guide to Total Reflection X-ray Fluorescence
Author: Martina Schmeling
Publisher: Elsevier
Total Pages: 0
Release: 2023-11-01
Genre: Science
ISBN: 9780323959155
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A Practical Guide to Total Reflection X-ray Fluorescence discusses how a wide range of samples can be analyzed using Total Reflection X-ray Fluorescence (TXRF) to obtain meaningful and accurate results. Sample handling is a complex problem and often very targeted approaches are needed. The strengths and weaknesses of the method are discussed in the context of each application in this book. This includes guidelines and suggestions of how to treat and analyze different samples and how to evaluate the data. In addition to sample handling, users of TXRF will learn how to use and calibrate the instrumentation, what specific features are present and which experimental parameters need to be considered, and how to evaluate the data.The book is divided into two parts. with the first part describing the theoretical aspects of the method and the second part being solely dedicated to its applications. The book emphasizes a practical approach to the method, including advantages and also limitations. The primary concept throughout the book is the chemical measurement process and how it applies to TXRF analysis. The concept is introduced in the first part of the book describing its main aspects like samples, sample handling, and quantification. In the second part of the book the topic is applied to the different application fields of TXRF, presented as separated chapters. Key case studies emphasizing the strength of the method are included in each of the chapters. The book also explains in detail the calibration of the instrument and method, experimental parameters to apply, quantification procedures, and spectra evaluation.This book serves as a valuable resource for users and users-to-be in the field of elemental and trace analysis. All co-authors offer extensive experience in the field of TXRF and can guide users through the chemical measurement process of a specific field of application including what elements are most suitable, and what issues may occur.

Handbook of Practical X-Ray Fluorescence Analysis

Handbook of Practical X-Ray Fluorescence Analysis
Author: Burkhard Beckhoff
Publisher: Springer Science & Business Media
Total Pages: 897
Release: 2007-05-18
Genre: Science
ISBN: 3540367225
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Download Handbook of Practical X-Ray Fluorescence Analysis Book in PDF, ePub and Kindle

X-Ray fluorescence analysis is an established technique for non-destructive elemental materials analysis. This book gives a user-oriented practical guidance to the application of this method. The book gives a survey of the theoretical fundamentals, analytical instrumentation, software for data processing, various excitation regimes including gracing incidents and microfocus measurements, quantitative analysis, applications in routine and micro analysis, mineralogy, biology, medicine, criminal investigations, archeology, metallurgy, abrasion, microelectronics, environmental air and water analysis. This book is the bible of X-Ray fluorescence analysis. It gives the basic knowledge on this technique, information on analytical equipment and guides the reader to the various applications. It appeals to researchers, analytically active engineers and advanced students.

Total-Reflection X-Ray Fluorescence Analysis and Related Methods

Total-Reflection X-Ray Fluorescence Analysis and Related Methods
Author: Reinhold Klockenkämper
Publisher: John Wiley & Sons
Total Pages: 554
Release: 2015-01-27
Genre: Science
ISBN: 1118460278
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Explores the uses of TXRF in micro- and trace analysis, and in surface- and near-surface-layer analysis • Pinpoints new applications of TRXF in different fields of biology, biomonitoring, material and life sciences, medicine, toxicology, forensics, art history, and archaeometry • Updated and detailed sections on sample preparation taking into account nano- and picoliter techniques • Offers helpful tips on performing analyses, including sample preparations, and spectra recording and interpretation • Includes some 700 references for further study

A Practical Guide for the Preparation of Specimens for X-Ray Fluorescence and X-Ray Diffraction Analysis

A Practical Guide for the Preparation of Specimens for X-Ray Fluorescence and X-Ray Diffraction Analysis
Author: Victor E. Buhrke
Publisher: Wiley-VCH
Total Pages: 0
Release: 1997-11-19
Genre: Science
ISBN: 9780471194583
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The first hands-on guide to XRD and XRF sampling and specimen preparation Systematic errors from poor sampling and improper specimen preparation can easily render X-ray diffraction (XRD) and X-ray fluorescence (XRF) data of questionable use for analysis. But, until now, the practical information that can help to reduce these errors has never been readily available in one volume. This book fills a vital gap in the literature, bringing together a wealth of material previously available only in workbooks, company manuals, and other inside sources. It provides detailed coverage of the major tasks involved in X-ray analysis - complete with theory, step-by-step methods, equipment suggestions, and problem-solving tips. With a full complement of tools and techniques, this comprehensive guide helps both beginners and experienced analysts to make the best decision on sample treatment and get accurate XRD and XRF results-saving valuable time, money, and effort. Covers X-ray techniques for analyzing biological, geological, metallic, ceramic, and other materials * Addresses all aspects of specimen preparation, including handling unusual or very small samples, liquids and solutions, and more * Features special chapters on specimen preparation equipment and XRF standards * Contains useful bibliography and helpful references.

X-Ray Fluorescence in Biological Sciences

X-Ray Fluorescence in Biological Sciences
Author: Vivek K. Singh
Publisher: John Wiley & Sons
Total Pages: 692
Release: 2022-03-28
Genre: Science
ISBN: 1119645549
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X-Ray Fluorescence in Biological Sciences Discover a comprehensive exploration of X-ray fluorescence in chemical biology and the clinical and plant sciences In X-Ray Fluorescence in Biological Sciences: Principles, Instrumentation, and Applications, a team of accomplished researchers delivers extensive coverage of the application of X-ray fluorescence (XRF) in the biological sciences, including chemical biology, clinical science, and plant science. The book also explores recent advances in XRF imaging techniques in these fields. The authors focus on understanding and investigating the intercellular structures and metals in plant cells, with advanced discussions of recently developed micro-analytical methods, like energy dispersive X-ray fluorescence spectrometry (EDXRF), total reflection X-ray fluorescence spectrometry (TXRF), micro-proton induced X-ray emission (micro-PIXE), electron probe X-ray microanalysis (EPXMA), synchrotron-based X-ray fluorescence microscopy (SXRF, SRIXE, or micro-XRF) and secondary ion mass spectrometry (SIMS). With thorough descriptions of protocols and practical approaches, the book also includes: A thorough introduction to the historical background and fundamentals of X-ray fluorescence, as well as recent developments in X-ray fluorescence analysis Comprehensive explorations of the general properties, production, and detection of X-rays and the preparation of samples for X-ray fluorescence analysis Practical discussions of the quantification of prepared samples observed under X-ray fluorescence and the relation between precision and beam size and sample amount In-depth examinations of wavelength-dispersive X-ray fluorescence and living materials Perfect for students and researchers studying the natural and chemical sciences, medical biology, plant physiology, agriculture, and botany, X-Ray Fluorescence in Biological Sciences: Principles, Instrumentation, and Applications will also earn a place in the libraries of researchers at biotechnology companies.

A Practical Guide to Graphite Furnace Atomic Absorption Spectrometry

A Practical Guide to Graphite Furnace Atomic Absorption Spectrometry
Author: David J. Butcher
Publisher: John Wiley & Sons
Total Pages: 282
Release: 1998-03-23
Genre: Science
ISBN: 9780471125532
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Die Atomabsorptionsspektroskopie mit Graphitrohrküvetten wird vor allem in der Material- und Umweltwissenschaft zur Untersuchung von Legierungen, Keramiken, Polymeren, Kompositwerkstoffen und Abwässern eingesetzt. Dieses umfangreiche Handbuch enthält viele praktische Beispiele, Tips und Tricks sowie Angaben zur instrumentellen Ausrüstung, zu modernen Entwicklungen und zur Fehlersuche: Eine wahre Fundgrube für den Praktiker, jedoch auch für Einsteiger geeignet - mit verschiedenen Anhängen, historischen Hintergrundinformationen, Literaturverzeichnissen und einem Glossar der verwendeten Fachterminologie. (06/98)

Practical Guide To Chemometrics

Practical Guide To Chemometrics
Author: Paul Gemperline
Publisher: CRC Press
Total Pages: 552
Release: 2006-04-16
Genre: Mathematics
ISBN: 1420018302
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The limited coverage of data analysis and statistics offered in most undergraduate and graduate analytical chemistry courses is usually focused on practical aspects of univariate methods. Drawing in real-world examples, Practical Guide to Chemometrics, Second Edition offers an accessible introduction to application-oriented multivariate meth

X-Ray Fluorescence Spectrometry and Related Techniques

X-Ray Fluorescence Spectrometry and Related Techniques
Author: Eva Margui
Publisher: Momentum Press
Total Pages: 149
Release: 2013-01-25
Genre: Technology & Engineering
ISBN: 1606503936
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X-ray fluorescence spectrometry (XRF) is a well-established analytical technique for qualitative and quantitative elemental analysis of a wide variety of routine quality control and research samples. Among its many desirable features, it delivers true multi-element character analysis, acceptable speed and economy, easy of automation, and the capacity to analyze solid samples. This remarkable contribution to this field provides a comprehensive and up-to-date account of basic principles, recent developments, instrumentation, sample preparation procedures, and applications of XRF analysis. If you are a professional in materials science, analytic chemistry, or physics, you will benefit from not only the review of basics, but also the newly developed technologies with XRF. Those recent technological advances, including the design of low-power micro- focus tubes and novel X-ray optics and detectors, have made it possible to extend XRF to the analysis of low-Z elements and to obtain 2D or 3D information on a micrometer-scale. And, the recent development and commercialization of bench top and portable instrumentation, offering extreme simplicity of operation in a low-cost design, have extended the applications of XRF to many more analytical problems.

A Practical Guide to Geometric Regulation for Distributed Parameter Systems

A Practical Guide to Geometric Regulation for Distributed Parameter Systems
Author: Eugenio Aulisa
Publisher: CRC Press
Total Pages: 1266
Release: 2015-06-18
Genre: Mathematics
ISBN: 1420061356
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A Practical Guide to Geometric Regulation for Distributed Parameter Systems provides an introduction to geometric control design methodologies for asymptotic tracking and disturbance rejection of infinite-dimensional systems. The book also introduces several new control algorithms inspired by geometric invariance and asymptotic attraction for a wide range of dynamical control systems. The first part of the book is devoted to regulation of linear systems, beginning with the mathematical setup, general theory, and solution strategy for regulation problems with bounded input and output operators. The book then considers the more interesting case of unbounded control and sensing. Mathematically, this case is more complicated and general theorems in this area have become available only recently. The authors also provide a collection of interesting linear regulation examples from physics and engineering. The second part focuses on regulation for nonlinear systems. It begins with a discussion of theoretical results, characterizing solvability of nonlinear regulator problems with bounded input and output operators. The book progresses to problems for which the geometric theory based on center manifolds does not directly apply. The authors show how the idea of attractive invariance can be used to solve a series of increasingly complex regulation problems. The book concludes with the solutions of challenging nonlinear regulation examples from physics and engineering.

X-Ray Fluorescence Spectrometry and Its Applications to Archaeology

X-Ray Fluorescence Spectrometry and Its Applications to Archaeology
Author: Mary Kate Donais
Publisher: Momentum Press
Total Pages: 217
Release: 2018-05-30
Genre: Technology & Engineering
ISBN: 1944749306
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This book serves as a practical guide for applications of X-ray fluorescence spectrometry, a nondestructive elemental analysis technique, to the study and understanding of archaeology. Descriptions of XRF theory and instrumentation and an introduction to field applications and practical aspects of archaeology provide new users to XRF and/or new to archaeology with a solid foundation on which to base further study. Considering recent trends within field archaeology, information specific to portable instrumentation also is provided. Discussions of qualitative and quantitative approaches and applications of statistical methods relate back to types of archaeological questions answerable through XRF analysis. Numerous examples, figures, and spectra from the authors’ field work are provided including chapters specific to pigments, ceramics, glass, construction materials, and metallurgical materials.