Synthesis Methods And Crystallization PDF Download
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| Author | : Riadh Marzouki |
| Publisher | : BoD – Books on Demand |
| Total Pages | : 138 |
| Release | : 2020-10-07 |
| Genre | : Technology & Engineering |
| ISBN | : 1838802231 |
Download Synthesis Methods and Crystallization Book in PDF, ePub and Kindle
New crystalline materials (organic, inorganic, hybrid) are promising for various applications, including electrical, piezoelectric, ferroelectric, magnetic, and catalytic processes. In addition, given their remarkable structural richness, these materials exhibit several interesting physical properties, such as ionic conduction, ion exchange, and others. Crystal growth, morphology, and grain size are factors influencing these physical properties. This book examines methods of synthesis of the most common crystalline materials and describes nucleation and crystal growth of various materials.
| Author | : Xinwen Guo |
| Publisher | : |
| Total Pages | : 0 |
| Release | : 2019 |
| Genre | : Electronic books |
| ISBN | : |
Download Synthesis Methods and Crystallization of MOFs Book in PDF, ePub and Kindle
Metal-organic frameworks (MOFs) are a class of porous crystalline materials constructed of metal centres with organic linkers, creating one-, two-, or three-dimensional well-organized frameworks with very high surface areas. The study of MOFs has become one of the research hot spots in many fields, owing to the broad potential applications projected for these materials in various areas. It is well recognized that synthesis strategies dictate the structure and thus the properties and performance of the resulted MOFs. This chapter provides a comprehensive up-to-date overview on the modulated synthesis strategies for MOFs. The ability to control crystal morphology and size by a number of modulated synthesis methods is illustrated by the zirconium-terephthalate-based MOF, the UiO-66, and a number of other MOFs.
| Author | : Edward Tiekink |
| Publisher | : Walter de Gruyter GmbH & Co KG |
| Total Pages | : 421 |
| Release | : 2017-11-20 |
| Genre | : Science |
| ISBN | : 3110463792 |
Download Multi-Component Crystals Book in PDF, ePub and Kindle
In this volume, contributions covering the theoretical and practical aspects of multicomponent crystals provide a timely and contemporary overview of the state-of-the art of this vital aspect of crystal engineering/materials science. With a solid foundation in fundamentals, multi-component crystals can be formed, for example, to enhance pharmaceutical properties of drugs, for the specific control of optical responses to external stimuli and to assemble molecules to allow chemical reactions that are generally intractable following conventional methods. Contents Pharmaceutical co-crystals: crystal engineering and applications Pharmaceutical multi-component crystals: improving the efficacy of anti-tuberculous agents Qualitative and quantitative crystal engineering of multi-functional co-crystals Control of photochromism in N-salicylideneaniline by crystal engineering Quinoline derivatives for multi-component crystals: principles and applications N-oxides in multi-component crystals and in bottom-up synthesis and applications Multi-component crystals and non-ambient conditions Co-crystals for solid-state reactivity and thermal expansion Solution co-crystallisation and its applications The salt-co-crystal continuum in halogen-bonded systems Large horizontal displacements of benzene-benzene stacking interactions in co-crystals Simultaneous halogen and hydrogen bonding to carbonyl and thiocarbonylfunctionality Crystal chemistry of the isomeric N,N’-bis(pyridin-n-ylmethyl)-ethanediamides, n = 2, 3 or 4 Solute・solvent interactions mediated by main group element (lone-pair)・・・π(aryl) interactions
| Author | : Paul Hagenmuller |
| Publisher | : Elsevier |
| Total Pages | : 621 |
| Release | : 2012-12-02 |
| Genre | : Science |
| ISBN | : 0323144365 |
Download Preparative Methods in Solid State Chemistry Book in PDF, ePub and Kindle
Preparative Methods in Solid State Chemistry deals with the preparative methods used in solid state chemistry and highlights the importance of the chemist's role in preparing materials of desired quality as well as obtaining materials according to the requirements of the user such as the physicist. Topics covered range from high-pressure techniques in preparative chemistry to methods of growing single crystals of high-melting-point oxides. This book is comprised of 14 chapters and begins with an overview of possibilities for high-pressure synthesis, as well as the methods used to obtain high pressures, including transmission by gaseous or liquid fluids or in the solid state. The method of shock waves is then considered both from the point of view of thermodynamics and thermoelasticity, along with the possibility of using superpressures for evidently revolutionary applications. Subsequent chapters focus on the synthesis of single crystals of refractory oxides either at high temperatures (essentially liquid-solid transformations) or at lower temperatures in the presence of a solvent or a chemical reagent. The production of single crystals by electrolytic reduction in molten salts is also described. Numerous examples of vapor transport reactions in a temperature gradient are presented. This monograph should be of interest to chemists and students of solid state chemistry.
| Author | : Dario Braga |
| Publisher | : John Wiley & Sons |
| Total Pages | : 362 |
| Release | : 2007-02-27 |
| Genre | : Science |
| ISBN | : 3527609652 |
Download Making Crystals by Design Book in PDF, ePub and Kindle
An excellent overview of the manifold aspects of modern crystal engineering. From design and preparation to spectroscopy and applications, this handbook both covers and evaluates all aspects of crystal engineering. Clearly structured, it provides an overview of the current status as seen from its various angles as well as a comparison of different techniques and applications. An essential source of high quality information for everyone working in this booming and interdisciplinary field: spectroscopists, physical and inorganic chemists as well as materials scientists working in nanotechnology and the pharmaceutical industry.
| Author | : K. Lal |
| Publisher | : Elsevier |
| Total Pages | : 583 |
| Release | : 2012-12-02 |
| Genre | : Technology & Engineering |
| ISBN | : 008098469X |
Download Synthesis, Crystal Growth and Characterization Book in PDF, ePub and Kindle
Synthesis, Crystal Growth and Characterization presents the proceedings of the International School on Synthesis, Crystal Growth and Characterization of Materials for Energy Conversion and Storage, held on October 12-23, 1981, at the National Physical Laboratory in New Delhi, India. The book consists of lectures by distinguished scientists from around the world who tackle different aspects of synthesis, crystal growth, characterization of materials, energy conversion, and energy storage. Organized into four parts encompassing 26 chapters, the book begins with an overview of the synthesis of materials at high temperatures and pressures before turning to a discussion of how macrocrystalline and amorphous silicon is prepared. It then looks at fundamental principles underlying the process of crystal growth, both from the vapor phase and from melt, and methodically introduces the reader to the different techniques used to characterize materials, including neutron scattering and electron transport. The next chapters focus on point defects and aggregates that influence the critical electronic properties of semiconducting materials, X-ray diffraction studies of strains and stresses in thin films used in solid-state devices, and electron spectroscopic studies of solid surfaces. The book also considers the role of physics in microelectronics and vice versa, fast ion transport in solids, and the concept of Syadvada in relation to modern physics. This volume is a valuable resource for participants of the International School on Synthesis, Crystal Growth and Characterization of Materials for Energy Conversion and Storage, as well as active researchers working in areas related to the field.
| Author | : Marcello Andreeta |
| Publisher | : BoD – Books on Demand |
| Total Pages | : 582 |
| Release | : 2012-09-19 |
| Genre | : Science |
| ISBN | : 9535107577 |
Download Crystallization Book in PDF, ePub and Kindle
Crystallization is one of the most ancient and interdisciplinary topics of research known to mankind. Crystals can be organic or inorganic and may be produced from melts, liquid solutions, vapors or even in solid state. Notwithstanding its inherently high complexity, the crystallization process is part of our everyday lives, from ice making in our homes to the most state-of-the-art chemical and electronic industry. In this book, our purpose was to present new insights to the reader, as well as crucial and very useful information for researchers working in this field, while simultaneously creating a comprehensive text about crystallization processes which may serve as a starting point for people with different backgrounds.
| Author | : Yitzhak Mastai |
| Publisher | : BoD – Books on Demand |
| Total Pages | : 672 |
| Release | : 2012-04-27 |
| Genre | : Science |
| ISBN | : 9535105817 |
Download Advances in Crystallization Processes Book in PDF, ePub and Kindle
Crystallization is used at some stage in nearly all process industries as a method of production, purification or recovery of solid materials. In recent years, a number of new applications have also come to rely on crystallization processes such as the crystallization of nano and amorphous materials. The articles for this book have been contributed by the most respected researchers in this area and cover the frontier areas of research and developments in crystallization processes. Divided into five parts this book provides the latest research developments in many aspects of crystallization including: chiral crystallization, crystallization of nanomaterials and the crystallization of amorphous and glassy materials. This book is of interest to both fundamental research and also to practicing scientists and will prove invaluable to all chemical engineers and industrial chemists in the process industries as well as crystallization workers and students in industry and academia.
| Author | : Jiri Cejka |
| Publisher | : John Wiley & Sons |
| Total Pages | : 918 |
| Release | : 2010-05-27 |
| Genre | : Technology & Engineering |
| ISBN | : 9783527630301 |
Download Zeolites and Catalysis Book in PDF, ePub and Kindle
This indispensable two-volume handbook covers everything on this hot research field. The first part deals with the synthesis, modification, characterization and application of catalytic active zeolites, while the second focuses on such reaction types as cracking, hydrocracking, isomerization, reforming and other industrially important topics. Edited by a highly experienced and internationally renowned team with chapters written by the "Who's Who" of zeolite research.
| Author | : Hsien-Hsin Tung |
| Publisher | : John Wiley & Sons |
| Total Pages | : 304 |
| Release | : 2009-06-17 |
| Genre | : Science |
| ISBN | : 0470447788 |
Download Crystallization of Organic Compounds Book in PDF, ePub and Kindle
Filled with industrial examples emphasizing the practical applications of crystallization methodologies Based on the authors' hands-on experiences as process engineers at Merck, Crystallization of Organic Compounds guides readers through the practical aspects of crystallization. It uses plenty of case studies and examples of crystallization processes, ranging from development through manufacturing scale-up. The book not only emphasizes strategies that have been proven successful, it also helps readers avoid common pitfalls that can render standard procedures unsuccessful. The goal of this text is twofold: Build a deeper understanding of the fundamental properties of crystallization as well as the impact of these properties on crystallization process development. Improve readers' problem-solving abilities by using actual industrial examples with real process constraints. Crystallization of Organic Compounds begins with detailed discussions of fundamental thermodynamic properties, nucleation and crystal growth kinetics, process dynamics, and scale-up considerations. Next, it investigates modes of operation, including cooling, evaporation, anti-solvent, and reactive crystallization. The authors conclude with special applications such as ultrasound in crystallization and computational fluid dynamics in crystallization. Most chapters feature multiple examples that guide readers step by step through the crystallization of active pharmaceutical ingredients (APIs). With its focus on industrial applications, this book is recommended for chemical engineers and chemists who are involved with the development, scale-up, or operation of crystallization processes in the pharmaceutical and fine chemical industries.
