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Author | : Roy H. Bible |
Publisher | : Springer Science & Business Media |
Total Pages | : 154 |
Release | : 2013-11-11 |
Genre | : Science |
ISBN | : 1468482882 |
Download Interpretation of NMR Spectra Book in PDF, ePub and Kindle
In writing this book I had two main objectives: (1) to teach the organic chemist how to interpret proton magnetic resonance spectra, and (2) to provide the reference data which are constantly needed in the use of proton spectra. I have felt that it was im portant to point out not only the information which can be gained from spectra, but also the limitations and the potential pitfalls. All of the important facts are organized into tabular summaries. Every effort has been made to present the material clearly, con cisely, completely, and accurately. At the same time, subjects not directly related to the interpretation of spectra have been omitted. Thus, while the conclusions drawn from theory are presented, the theory itself has been avoided. There are a number of advantages in learning the empirical facts before learning the theory. First of all, in interpreting spectra one usually has to rely on his knowledge of the accumulated empirical correlations much more than on his knowledge of the theory. In fact, one could know all of the theory and still not b~ able to interpret spectra unless he also knew the empirical facts. Secondly, the theory is much more easilyunderstoodafter the facts have been mastered.
Author | : Neil E. Jacobsen |
Publisher | : John Wiley & Sons |
Total Pages | : 1003 |
Release | : 2016-10-21 |
Genre | : Science |
ISBN | : 1119176883 |
Download NMR Data Interpretation Explained Book in PDF, ePub and Kindle
Through numerous examples, the principles of the relationship between chemical structure and the NMR spectrum are developed in a logical, step-by-step fashion Includes examples and exercises based on real NMR data including full 600 MHz one- and two-dimensional datasets of sugars, peptides, steroids and natural products Includes detailed solutions and explanations in the text for the numerous examples and problems and also provides large, very detailed and annotated sets of NMR data for use in understanding the material Describes both simple aspects of solution-state NMR of small molecules as well as more complex topics not usually covered in NMR books such as complex splitting patterns, weak long-range couplings, spreadsheet analysis of strong coupling patterns and resonance structure analysis for prediction of chemical shifts Advanced topics include all of the common two-dimensional experiments (COSY, ROESY, NOESY, TOCSY, HSQC, HMBC) covered strictly from the point of view of data interpretation, along with tips for parameter settings
Author | : Neil E. Jacobsen |
Publisher | : John Wiley & Sons |
Total Pages | : 652 |
Release | : 2016-10-21 |
Genre | : Science |
ISBN | : 1119047145 |
Download NMR Data Interpretation Explained Book in PDF, ePub and Kindle
Through numerous examples, the principles of the relationship between chemical structure and the NMR spectrum are developed in a logical, step-by-step fashion Includes examples and exercises based on real NMR data including full 600 MHz one- and two-dimensional datasets of sugars, peptides, steroids and natural products Includes detailed solutions and explanations in the text for the numerous examples and problems and also provides large, very detailed and annotated sets of NMR data for use in understanding the material Describes both simple aspects of solution-state NMR of small molecules as well as more complex topics not usually covered in NMR books such as complex splitting patterns, weak long-range couplings, spreadsheet analysis of strong coupling patterns and resonance structure analysis for prediction of chemical shifts Advanced topics include all of the common two-dimensional experiments (COSY, ROESY, NOESY, TOCSY, HSQC, HMBC) covered strictly from the point of view of data interpretation, along with tips for parameter settings
Author | : Antonio Randazzo |
Publisher | : Loghia Di Amoresano Claudia |
Total Pages | : 344 |
Release | : 2018 |
Genre | : Medical |
ISBN | : 9788895122403 |
Download Guide to Nmr Spectral Interpretation Book in PDF, ePub and Kindle
This book is designed to provide undergraduate and graduate students with practical strategies, methods and explanations to interpret the NMR spectra of small organic molecules. In particular, it is organized in a way that basic 1H- and 13iNMR concepts are introduced and immediately applied in a number of problems, solved and discussed in a step-by-step fashion. It contains almost exclusively real NMR data and it describes how to interpret the chemical shift, intensity and splitting pattern of the proton and carbon NMR signals (Chapters 1-5), paying attention to the effects of the magnetically non-equivalent nuclei (Chapter 4). The role of the solvent is also explained (Chapter 6), and a description of the interpretation of the most common two-dimensional NMR experiments is reported in Chapter 7. Chapter 8 is dedicated to the strategy for structural elucidation, while Chapter 9 contains exclusively summary problems.
Author | : James Keeler |
Publisher | : John Wiley & Sons |
Total Pages | : 533 |
Release | : 2011-09-19 |
Genre | : Science |
ISBN | : 1119964938 |
Download Understanding NMR Spectroscopy Book in PDF, ePub and Kindle
This text is aimed at people who have some familiarity with high-resolution NMR and who wish to deepen their understanding of how NMR experiments actually ‘work’. This revised and updated edition takes the same approach as the highly-acclaimed first edition. The text concentrates on the description of commonly-used experiments and explains in detail the theory behind how such experiments work. The quantum mechanical tools needed to analyse pulse sequences are introduced set by step, but the approach is relatively informal with the emphasis on obtaining a good understanding of how the experiments actually work. The use of two-colour printing and a new larger format improves the readability of the text. In addition, a number of new topics have been introduced: How product operators can be extended to describe experiments in AX2 and AX3 spin systems, thus making it possible to discuss the important APT, INEPT and DEPT experiments often used in carbon-13 NMR. Spin system analysis i.e. how shifts and couplings can be extracted from strongly-coupled (second-order) spectra. How the presence of chemically equivalent spins leads to spectral features which are somewhat unusual and possibly misleading, even at high magnetic fields. A discussion of chemical exchange effects has been introduced in order to help with the explanation of transverse relaxation. The double-quantum spectroscopy of a three-spin system is now considered in more detail. Reviews of the First Edition “For anyone wishing to know what really goes on in their NMR experiments, I would highly recommend this book” – Chemistry World “...I warmly recommend for budding NMR spectroscopists, or others who wish to deepen their understanding of elementary NMR theory or theoretical tools” – Magnetic Resonance in Chemistry
Author | : Roman Valiulin |
Publisher | : Walter de Gruyter GmbH & Co KG |
Total Pages | : 202 |
Release | : 2019-10-08 |
Genre | : Science |
ISBN | : 3110608464 |
Download NMR Multiplet Interpretation Book in PDF, ePub and Kindle
A visual guide for the interpretation of complex 1H-NMR spectra with a concise and illustrative practice problems section. This book is an easy-to-grasp source for (organic) chemists and students that want to understand and practice NMR spectroscopy.
Author | : Neil E. Jacobsen |
Publisher | : John Wiley & Sons |
Total Pages | : 640 |
Release | : 2007-09-10 |
Genre | : Science |
ISBN | : 0470173343 |
Download NMR Spectroscopy Explained Book in PDF, ePub and Kindle
NMR Spectroscopy Explained : Simplified Theory, Applications and Examples for Organic Chemistry and Structural Biology provides a fresh, practical guide to NMR for both students and practitioners, in a clearly written and non-mathematical format. It gives the reader an intermediate level theoretical basis for understanding laboratory applications, developing concepts gradually within the context of examples and useful experiments. Introduces students to modern NMR as applied to analysis of organic compounds. Presents material in a clear, conversational style that is appealing to students. Contains comprehensive coverage of how NMR experiments actually work. Combines basic ideas with practical implementation of the spectrometer. Provides an intermediate level theoretical basis for understanding laboratory experiments. Develops concepts gradually within the context of examples and useful experiments. Introduces the product operator formalism after introducing the simpler (but limited) vector model.
Author | : Roy H. Bible |
Publisher | : |
Total Pages | : 166 |
Release | : 2014-01-15 |
Genre | : |
ISBN | : 9781468482898 |
Download Interpretation of NMR Spectra Book in PDF, ePub and Kindle
Author | : Metin Balci |
Publisher | : Elsevier |
Total Pages | : 441 |
Release | : 2005-01-19 |
Genre | : Science |
ISBN | : 0080525539 |
Download Basic 1H- and 13C-NMR Spectroscopy Book in PDF, ePub and Kindle
Nuclear Magnetic Resonance (NMR) spectroscopy is a powerful and theoretically complex analytical tool. Basic 1H- and 13C-NMR Spectroscopy provides an introduction to the principles and applications of NMR spectroscopy. Whilst looking at the problems students encounter when using NMR spectroscopy, the author avoids the complicated mathematics that are applied within the field. Providing a rational description of the NMR phenomenon, this book is easy to read and is suitable for the undergraduate and graduate student in chemistry. Describes the fundamental principles of the pulse NMR experiment and 2D NMR spectra Easy to read and written with the undergraduate and graduate chemistry student in mind Provides a rational description of NMR spectroscopy without complicated mathematics
Author | : LeRoy F. Johnson |
Publisher | : |
Total Pages | : 117 |
Release | : 1977 |
Genre | : |
ISBN | : |
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