Cold Trappings And Reinjection Techniques For Gas Chromatography Mass Spectrometry PDF Download

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Split and Splitless Injection for Quantitative Gas Chromatography

Split and Splitless Injection for Quantitative Gas Chromatography
Author: Konrad Grob
Publisher: John Wiley & Sons
Total Pages: 480
Release: 2008-11-21
Genre: Science
ISBN: 3527612882

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This comprehensive and unique handbook of split and splitless injection techniques has been completely revised and updated. This new edition offers: - New insights concerning sample evaporation in the injector - Information about matrix effects - A new chapter on injector design The real processes within the injector are for the first time visualized and explained by the CD-ROM included in the book. Furthermore the reader will understand the concepts of injection techniques and get a knowledge of the sources of error. The handbook also includes many practical guidelines. From reviews of former editions: "This substantial book is on injection techniques alone, which ... demonstrates this can have many pitfalls ... no one should be allowed to direct a laboratory doing quantitative analysis by GC without first being thoroughly familar with this book ..." The Analyst "This is a detailed reference volume filled with practical suggestions and techniques for managing split and splitless injection in the day-to-day world of the working gas chromatographer. It will be useful ... for anyone who must work hands-on with GC." Journal of High Resolution Chromatography


GC Inlets

GC Inlets
Author: Matthew S. Klee
Publisher: Hewlett-Packard, Avondale Division
Total Pages: 132
Release: 1990-02-01
Genre: Gas chromatography
ISBN: 9781880313008

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Solid Fuels and Heavy Hydrocarbon Liquids: Thermal Characterization and Analysis

Solid Fuels and Heavy Hydrocarbon Liquids: Thermal Characterization and Analysis
Author: Rafael Kandiyoti
Publisher: Elsevier
Total Pages: 365
Release: 2006-04-06
Genre: Science
ISBN: 0080463606

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The first strand involves a critical overview of the design of experimental methods used for examining the thermal behaviour of solid fuels [pyrolysis, liquefaction and gasification], while the second will emphasise chemical structures and molecular mass distributions of coal derived tars, extracts and pitches, petroleum-derived asphaltenes, and biomass derived heavy hydrocarbon liquids.Two major, interdependent strands in the study of fossil and renewable fuel utilisation are focused on within this text:(i) Thermal characterisation of solid fuels including various ranks of coals, biomass and waste, and, (ii) The analytical characterisation of heavy hydrocarbon liquids, covering coal, petroleum and biomass derived heavy fractions. Two major, interdependent strands in the study of fossil and renewable fuel utilisation are focused on within this text: (i) Thermal characterisation of solid fuels including various ranks of coals, biomass and waste, and, (ii) The analytical characterisation of heavy hydrocarbon liquids, covering coal, petroleum and biomass derived heavy fractions.


Basic Gas Chromatography-Mass Spectrometry

Basic Gas Chromatography-Mass Spectrometry
Author: F.W. Karasek
Publisher: Elsevier
Total Pages: 210
Release: 2012-12-02
Genre: Science
ISBN: 0080929060

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The book begins by covering the basic principles of both gas chromatography (GC) and mass spectrometry (MS) to the extent necessary to understand and deal with the data generated in a GC-MS analysis. The focus then turns to the particular requirements created by a direct combination of these two techniques into a single instrumentation system. The data generated and their use are covered in detail. The role of the computer and its specific software receives special attention, especially in the matter of compound identification via mass spectral search techniques. GC-MS-computer instrumentation has reached such a plateau of excellence today that the present commercial systems will not be obsolete for a long time to come. Therefore, a detailed description of these systems is not only informative but is also pertinent to the subject matter of this book. Finally, representative applications and results obtained with GC-MS-computer techniques are presented and chosen in such a way as to permit extrapolation of specific applications to similar problems encountered by the reader. To aid the reader in mastering the subject matter and increase understanding, interpretation problems and suggested readings are included. The format is instructional, informative and application-oriented with material presented in such a way as to be useful to a broad spectrum of people.The book serves as a text in its own right.The software package Gas Chromatography-Mass Spectrometry: A Knowledge Base, by F.A. Settle, Jr. and M.A. Pleva provides rapid access to a wealth of current information in the GC-MS field. Its three diskettes (51/4 inch) allow the user three ways to access: the index mode, the tree mode and a keyword search mode. The package may be purchased separately and is available for the IBM-PC and compatibles.The software provides a valuable supplement to the book.


Gas Chromatography

Gas Chromatography
Author: Peter Kusch
Publisher: BoD – Books on Demand
Total Pages: 144
Release: 2019-09-04
Genre: Science
ISBN: 1838818650

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Gas chromatography (GC) is one of the most important types of chromatography used in analytical chemistry for separating and analyzing chemical organic compounds. Today, gas chromatography is one of the most widespread investigation methods of instrumental analysis. This technique is used in the laboratories of chemical, petrochemical, and pharmaceutical industries, in research institutes, and also in clinical, environmental, and food and beverage analysis. This book is the outcome of contributions by experts in the field of gas chromatography and includes a short history of gas chromatography, an overview of derivatization methods and sample preparation techniques, a comprehensive study on pyrazole mass spectrometric fragmentation, and a GC/MS/MS method for the determination and quantification of pesticide residues in grape samples.


Gas Chromatography Mass Spectrometry Applications in Microbiology

Gas Chromatography Mass Spectrometry Applications in Microbiology
Author: Goran Odham
Publisher: Springer Science & Business Media
Total Pages: 452
Release: 2013-11-11
Genre: Science
ISBN: 146844526X

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During recent years there has been increasing interest in the value of a number of chemical and physical-chemical analytical methods for the detection and characterization of microorganisms. Furthermore, such methods are currently used in studies on microbial metabolic processes, on the role of microorganisms in the turnover of inorganic and organic compounds, and on the impact on environmental changes by microbial activity. Moreover, the introduction of some of these methods not only shortens the analytical time period compared to ·'traditional" techniques, but also improves the analytical quality. Mass spectrometry (MS) combined with chromatographic inlet systems, particularly gas chromatography (GC), belongs to those methods which during recent years have established their value for the above-mentioned purposes. The present volume starts with basic chapters on the principles for MS and common inlet systems, particulary Gc. It discusses applications of these techniques to a number of microbiological disciplines, e.g., ecologi cal and medical microbiology. Emphasis is laid on organic compound classes vii viii / PREFACE of special relevance to microbiology, e.g., volatiles, lipids, amino acids, peptides and carbohydrates. Some compound classes of a more general biochemical rather than specific microbiological importance, e.g., steroids and nucleotides, are dealt with briefly. The editors wish to thank all those who have contributed to this book. We hope it will stimulate further research in this futuristic field and will be of practical value.


Gas Chromatography/Mass Spectrometry

Gas Chromatography/Mass Spectrometry
Author: Hans-Ferdinand Linskens
Publisher: Springer Science & Business Media
Total Pages: 321
Release: 2012-12-06
Genre: Science
ISBN: 3642826121

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Modern Methods of Plant Analysis When the handbook Modern Methods of Plant Analysis was first introduced in 1954 the considerations were: 1. the dependence of scientific progress in biology on the improvement of existing and the introduction of new methods; 2. the difficulty in finding many new analytical methods in specialized journals which are normally not accessible to experimental plant biologists; 3. the fact that in the methods sections of papers the description of methods is frequently so compact, or even sometimes so incomplete that it is difficult to reproduce experiments. These considerations still stand today. The series was highly successful, seven volumes appearing between 1956 and 1964. Since there is still today a demand for the old series, the publisher has decided to resume publication of Modern Methods of Plant Analysis. It is hoped that the New Series will be just as acceptable to those working in plant sciences and related fields as the early volumes undoubtedly were. It is difficult to single out the major reasons for success of any publication, but we believe that the methods published in the first series were up-to-date at the time and presented in a way that made description, as applied to plant material, complete in itself with little need to consult other publications. Contributing authors have attempted to follow these guidelines in this New Series of volumes.